NEW 2-DIMENSIONAL METHODS FOR DOUBLE-ROTATION EXPERIMENTS

被引:2
作者
AMOUREUX, JP
FERNANDEZ, C
DUMAZY, Y
机构
关键词
SOLID-STATE NMR; QUADRUPOLAR NUCLEI; DOR TECHNIQUE;
D O I
10.1051/jcp/1995921943
中图分类号
Q5 [生物化学]; Q7 [分子生物学];
学科分类号
071010 ; 081704 ;
摘要
We describe a new 2D high-resolution technique for nuclei with semi-integer spins subjected to strong quadrupole interactions. This VADOR (Variable Angle DOR) technique separates anisotropic spectral patterns according to the isotropic shift of each species. No sudden sample reorientation is needed for VADOR which can then be used regardless of the ''relaxation times''.
引用
收藏
页码:1943 / 1946
页数:4
相关论文
共 3 条
[1]   VARIABLE-ANGLE CORRELATION SPECTROSCOPY IN SOLID-STATE NUCLEAR-MAGNETIC-RESONANCE [J].
FRYDMAN, L ;
CHINGAS, GC ;
LEE, YK ;
GRANDINETTI, PJ ;
EASTMAN, MA ;
BARRALL, GA ;
PINES, A .
JOURNAL OF CHEMICAL PHYSICS, 1992, 97 (07) :4800-4808
[2]   TOWARDS HIGH-RESOLUTION NMR OF MORE NUCLEI IN SOLIDS - SAMPLE SPINNING WITH TIME-DEPENDENT SPINNER AXIS ANGLE [J].
LLOR, A ;
VIRLET, J .
CHEMICAL PHYSICS LETTERS, 1988, 152 (2-3) :248-253
[3]   HIGH-RESOLUTION SOLID-STATE NMR AVERAGING OF 2ND-ORDER EFFECTS BY MEANS OF A DOUBLE-ROTOR [J].
SAMOSON, A ;
LIPPMAA, E ;
PINES, A .
MOLECULAR PHYSICS, 1988, 65 (04) :1013-1018