APPLICATION OF 2-DIMENSIONAL SHIFT CORRELATED NMR TECHNIQUES TO THE STRUCTURE DETERMINATION OF AN UNUSUAL MARINE ALKALOID, ISOSARAINE-2

被引：13

作者：

CIMINO, G ^{[1
]}

FONTANA, A ^{[1
]}

MADAIO, A ^{[1
]}

SCOGNAMIGLIO, G ^{[1
]}

TRIVELLONE, E ^{[1
]}

机构：

[1] CNR,IST CHIM MOLEC INTERESSE BIOL,VIA TOIANO 6,I-80072 ARCO,ITALY

来源：

MAGNETIC RESONANCE IN CHEMISTRY | 1991年 / 29卷 / 04期

关键词：

SARAINES; 2D COSY NMR; 2D H-1 C-13 COSY NMR; ALKALOIDS; SPONGE; RENIERA-SARAI;

D O I：

10.1002/mrc.1260290408

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

An extensive application of two-dimensional proton-proton and proton-carbon shift correlated spectroscopy allowed the structural elucidation of isosaraiane-2, a minor component of an unique family of alkaloids from the sponge Reniera sarai.

引用

页码：327 / 332

页数：6

共 10 条

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[3] BRAEKMAN JC, 1982, TETRAHEDRON LETT, P4277
[4] CIMINO G, 1986, B SOC CHIM BELG, V95, P783
[5] AMAZING NEW ALKALOID SKELETONS FROM THE MARINE SPONGE RENIERA-SARAI
CIMINO, G
PULITI, R
SCOGNAMIGLIO, G
SPINELLA, A
TRIVELLONE, E
MATTIA, CA
MAZZARELLA, L
[J]. PURE AND APPLIED CHEMISTRY, 1989, 61 (03) : 535 - 538
[6] UNPRECEDENTED ALKALOID SKELETON FROM THE MEDITERRANEAN SPONGE RENIERA-SARAI - X-RAY STRUCTURE OF AN ACETATE DERIVATIVE OF SARAIN-A
CIMINO, G
MATTIA, CA
MAZZARELLA, L
PULITI, R
SCOGNAMIGLIO, G
SPINELLA, A
TRIVELLONE, E
[J]. TETRAHEDRON, 1989, 45 (12) : 3863 - 3872
[7] ISOSARAIN-1 - A NEW ALKALOID FROM THE MEDITERRANEAN SPONGE RENIERA-SARAI
CIMINO, G
SPINELLA, A
TRIVELLONE, E
[J]. TETRAHEDRON LETTERS, 1989, 30 (01) : 133 - 136
[8] ARAGUPETROSINE-A, A NEW VASODILATIVE MACROCYCLIC QUINOLIZIDINE ALKALOID FROM AN OKINAWAN MARINE SPONGE XESTOSPONGIA SP
KOBAYASHI, M
KAWAZOE, K
KITAGAWA, I
[J]. TETRAHEDRON LETTERS, 1989, 30 (31) : 4149 - 4152
[9] NAKAGAWA M, 1984, TETRAHEDRON LETT, P3227
[10] STOTHERS JB, 1972, ORGANIC CHEM CARBON, V24, P146

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