2-DIMENSIONAL J-SCALED SI-29 NMR COSY OF HIGHLY SILICEOUS MORDENITE

被引：21

作者：

KOLODZIEJSKI, W ^{[1
]}

BARRIE, PJ ^{[1
]}

HE, HY ^{[1
]}

KLINOWSKI, J ^{[1
]}

机构：

[1] UNIV CAMBRIDGE,DEPT CHEM,LENSFIELD RD,CAMBRIDGE CB2 1EW,ENGLAND

来源：

JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS | 1991年 / 14期

关键词：

D O I：

10.1039/c39910000961

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The two dimensional solid-state J-scaled COSY NMR spectrum of highly siliceous mordenite reveals the tetrahedral site connectivities, permitting the unambiguous assignment of the Si-29 spectrum.

引用

页码：961 / 962

页数：2

共 18 条

[1] ALUMINUM SITING IN MORDENITE AND DEALUMINATION MECHANISM [J].

BODART, P ;

NAGY, JB ;

DEBRAS, G ;

GABELICA, Z ;

JACOBS, PA .

JOURNAL OF PHYSICAL CHEMISTRY, 1986, 90 (21) :5183-5190

[2]

Breck D. W, 1974, ZEOLITE MOL SIEVES

[3]

ENGELHARDT G, 1989, RECENT ADV ZEOLITE S, V52, P151

[4]

Engelhardt G., 1987, HIGH RESOLUTION SOLI

[5] DETERMINATION OF 3-DIMENSIONAL LATTICE CONNECTIVITIES IN ZEOLITES USING NATURAL-ABUNDANCE SI-29 TWO-DIMENSIONAL NMR AND THE DIRECT OBSERVATION OF SI-29-O-SI-29 COUPLINGS [J].

FYFE, CA ;

GIES, H ;

FENG, Y ;

KOKOTAILO, GT .

NATURE, 1989, 341 (6239) :223-225

[6]

FYFE CA, 1984, J AM CHEM SOC, V106, P4435, DOI 10.1021/ja00328a024

[7] NATURAL-ABUNDANCE 2-DIMENSIONAL SI-29 MAS NMR INVESTIGATION OF THE 3-DIMENSIONAL BONDING CONNECTIVITIES IN THE ZEOLITE CATALYST ZSM-5 [J].

FYFE, CA ;

GRONDEY, H ;

FENG, Y ;

KOKOTAILO, GT .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1990, 112 (24) :8812-8820

[8] NATURAL-ABUNDANCE 2-DIMENSIONAL SOLID-STATE SI-29 NMR INVESTIGATIONS OF 3-DIMENSIONAL LATTICE CONNECTIVITIES IN ZEOLITE STRUCTURES [J].

FYFE, CA ;

FENG, Y ;

GIES, H ;

GRONDEY, H ;

KOKOTAILO, GT .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1990, 112 (09) :3264-3270

[9] 3-DIMENSIONAL LATTICE CONNECTIVITIES FROM TWO-DIMENSIONAL HIGH-RESOLUTION SOLID-STATE NMR - SI-29 MAS NMR INVESTIGATION OF THE SILICATE LATTICE OF ZEOLITE ZSM-39 (DODECASIL-3C) [J].

FYFE, CA ;

GIES, H ;

FENG, Y .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1989, 111 (20) :7702-7707

[10] DEMONSTRATION OF 3-DIMENSIONAL LATTICE CONNECTIVITIES IN ZEOLITES BY TWO-DIMENSIONAL HIGH-RESOLUTION SOLID-STATE NMR-SPECTROSCOPY [J].

FYFE, CA ;

GIES, H ;

FENG, Y .

JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS, 1989, (17) :1240-1242

← 1 2 →