SEPARATION AND ISOLATION OF VOLATILE ORGANIC-COMPOUNDS USING VACUUM DISTILLATION WITH GC/MS DETERMINATION

被引：26

作者：

HIATT, MH ^{[1
]}

YOUNGMAN, DR ^{[1
]}

DONNELLY, JR ^{[1
]}

机构：

[1] LOCKHEED ENVIRONM SYST & TECHNOL CO,LAS VEGAS,NV 89119

来源：

ANALYTICAL CHEMISTRY | 1994年 / 66卷 / 06期

关键词：

D O I：

10.1021/ac00078a023

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

Vacuum distillation of water, soil, oil, and fish samples is presented as an alternative technique for determining volatile organic compounds (VOCs). Analyses of samples containing VOCs and non-VOCs at 50 ppb concentrations were performed to evaluate method limitations. Analyte recoveries were found to relate closing with boiling point unless a compound's water solubility exceeded 5 g/L. Recovery, precision, and method detection limits for VOCs demonstrate this technology is appropriate for environmental samples.

引用

页码：905 / 908

页数：4

共 10 条

[1]

[Anonymous], 1988, METHODS DETERMINATIO

[2] OCCURRENCE OF ORGANOHALIDES IN CHLORINATED DRINKING WATERS [J].

BELLAR, TA ;

LICHTENBERG, JJ ;

KRONER, RC .

JOURNAL AMERICAN WATER WORKS ASSOCIATION, 1974, 66 (12) :703-706

[3]

BELLAR TA, 1974, J AM WATER WORKS ASS, V66, P739

[4] ANALYSIS OF FISH AND SEDIMENT FOR VOLATILE PRIORITY POLLUTANTS [J].

HIATT, MH .

ANALYTICAL CHEMISTRY, 1981, 53 (09) :1541-1543

[5] DETERMINATION OF VOLATILE ORGANIC-COMPOUNDS IN FISH SAMPLES BY VACUUM DISTILLATION AND FUSED-SILICA CAPILLARY GAS-CHROMATOGRAPHY MASS-SPECTROMETRY [J].

HIATT, MH .

ANALYTICAL CHEMISTRY, 1983, 55 (03) :506-516

[6] SIMPLE METHOD FOR CONCENTRATING VOLATILES IN WATER FOR GAS-CHROMATOGRAPHIC ANALYSIS BY VACUUM DISTILLATION [J].

KOZLOSKI, RP .

JOURNAL OF CHROMATOGRAPHY, 1985, 346 (OCT) :408-412

[7] A METHOD FOR QUANTITATIVE-DETERMINATION OF VOLATILE ORGANIC-COMPOUNDS IN MARINE MACROALGAE [J].

NEWMAN, KA ;

GSCHWEND, PM .

LIMNOLOGY AND OCEANOGRAPHY, 1987, 32 (03) :702-708

[8]

SHIREY RE, 1993, SUPELCO REP, V12

[9]

1992, US EPA SW846

[10]

1991, OML010 US EPA DOC

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