1,2,5-OXADIAZOLES SUBSTITUTED AT RING NITROGEN .1. SYNTHESIS AND STUDY OF 2-ETHYL-1,2,5-OXADIZAOL-3(2H)-ONES

被引：17

作者：

SHEREMETEV, AB

STRELENKO, YA

NOVIKOVA, TS

KHMELNITSKII, LI

机构：

[1] N.D.Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences

来源：

TETRAHEDRON | 1993年 / 49卷 / 26期

关键词：

D O I：

10.1016/S0040-4020(01)87956-4

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

The first representatives of the 2-alkyl-1,2,5-oxadiazol-3(2H)-ones have been synthesized by the alkylation of trimethylsilyl derivatives of 3-hydroxyfurazans using triethyl orthoformate. The compounds obtained are investigated by C-13, N-14, N-15 and O-17 NMR, MS, IR and UV.

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页码：5905 / 5914

页数：10

相关论文

共 28 条

[1]

BACHKOVSKY IP, 1980, UKR KHIM ZH+, V46, P637

[2] 1.3-DIPOLAR CYCLOADDITIONS .68. ADDITIONS OF NITRILE OXIDES TO CN-MULTIPLE BONDS [J].

BAST, K ;

MACK, W ;

HUISGEN, R ;

CHRISTL, M .

CHEMISCHE BERICHTE-RECUEIL, 1972, 105 (09) :2825-&

[3]

BERGMAN J, 1976, TETRAHEDRON LETT, P3611

[4]

BERGMAN J, 1976, TETRAHEDRON LETT, P3615

[5] UNSYMMETRICALLY SUBSTITUTED FUROXANS .7. A C-13 NMR-STUDY OF A SERIES OF ISOMERIC PAIRS OF FUROXANS AND THE STRUCTURE OF THE 2 ISOMERIC CHLORO-PHENYL-FUROXANS [J].

CALVINO, R ;

FRUTTERO, R ;

GASCO, A ;

MORTARINI, V ;

AIME, S .

JOURNAL OF HETEROCYCLIC CHEMISTRY, 1982, 19 (02) :427-430

[6] RATES OF N-METHYLATION OF 2-METHYLBENZOTRIAZOLE, 2,1,3-BENZOXADIZOLE, 2,1,3-BENZOTHIA(OR SELENA)DIAZOLE, 1,2,5-OXADIAZOLE AND 1,2,5-THIADIAZOLE [J].

DAVIS, M ;

DEADY, LW ;

HOMFELD, E .

AUSTRALIAN JOURNAL OF CHEMISTRY, 1974, 27 (09) :1917-1921

[7] THE CHEMISTRY OF FULMINIC ACID REVISED [J].

DESARLO, F ;

GUARNA, A ;

BRANDI, A ;

GOTI, A .

TETRAHEDRON, 1985, 41 (22) :5181-5185

[8]

DODGE FD, 1891, LIEBIGS ANN CHEM, V264, P179

[9] 1,3-DIPOLAR ADDITION OF FORMONITRILE OXIDE AND HYDROXYIMINOACETONITRILE OXIDE TO SOME OLEFINS - SYNTHESIS OF ISOXAZOLIDINO[2,3-B]-DELTA-3-1,2,5-OXADIAZOLINES [J].

FAJKOS, J ;

EDWARDS, JA .

JOURNAL OF HETEROCYCLIC CHEMISTRY, 1974, 11 (01) :63-67

[10] SYNTHESIS OF 2-S-DIOXO ISOSTERES OF PURINE AND PYRIMIDINE NUCLEOSIDES .2. [J].

FERNANDEZRESA, P ;

STUD, M .

JOURNAL OF HETEROCYCLIC CHEMISTRY, 1982, 19 (02) :305-307