PREPARATION OF OPTICALLY PURE PYRIDYL-1-ETHANOLS

被引：51

作者：

SEEMAYER, R ^{[1
]}

SCHNEIDER, MP ^{[1
]}

机构：

[1] BERG UNIV GESAMTHSCH WUPPERTAL,FACHBEREICH 9,W-5600 WUPPERTAL 1,GERMANY

来源：

TETRAHEDRON-ASYMMETRY | 1992年 / 3卷 / 07期

关键词：

D O I：

10.1016/S0957-4166(00)82175-8

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

Using a highly enantioselective lipase from Pseudomonas sp. (SAM II) all enantiomers of the isomeric pyridyl-1-ethanols (R)- and (S)- 1 - 3 were prepared in optically pure form both by enzymatic hydrolysis and esterification.

引用

页码：827 / 830

页数：4

共 17 条

[1] BUCCIARELLI M, 1983, SYNTHESIS-STUTTGART, P879
[2] CERVINKA O, 1973, COLLECT CZECH CHEM C, V38, P1358
[3] QUANTITATIVE-ANALYSES OF BIOCHEMICAL KINETIC RESOLUTIONS OF ENANTIOMERS
CHEN, CS
FUJIMOTO, Y
GIRDAUKAS, G
SIH, CJ
[J]. JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1982, 104 (25) : 7294 - 7299
[4] ALPHA-METHOXY-ALPHA-TRIFLUOROMETHYLPHENYLACETIC ACID, A VERSATILE REAGENT FOR DETERMINATION OF ENANTIOMERIC COMPOSITION OF ALCOHOLS AND AMINES
DALE, JA
DULL, DL
MOSHER, HS
[J]. JOURNAL OF ORGANIC CHEMISTRY, 1969, 34 (09) : 2543 - &
[5] OPTICALLY-ACTIVE NAPROXEN BY KINETIC RESOLUTION
FRANCK, A
RUCHARDT, C
[J]. CHEMISTRY LETTERS, 1984, (08) : 1431 - 1434
[6] GARTNER H, 1984, ANGEW CHEM INT EDIT, V23, P172
[7] PREPARATION AND ABSOLUTE STEREOCHEMISTRY OF ISOMERIC PYRIDYLETHANOLS AND THREO-DI(2-PYRIDYL)ETHANEDIOL
IMUTA, M
ZIFFER, H
[J]. JOURNAL OF ORGANIC CHEMISTRY, 1978, 43 (18) : 3530 - 3532
[8] A HIGHLY SELECTIVE ESTER HYDROLASE FROM PSEUDOMONAS SP FOR THE ENZYMATIC PREPARATION OF ENANTIOMERICALLY PURE SECONDARY ALCOHOLS - CHIRAL AUXILIARIES IN ORGANIC-SYNTHESIS
LAUMEN, K
SCHNEIDER, MP
[J]. JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS, 1988, (09) : 598 - 600
[9] ENZYMIC PREPARATION OF ENANTIOMERICALLY PURE SECONDARY ALCOHOLS - ESTER SYNTHESIS BY IRREVERSIBLE ACYL TRANSFER USING A HIGHLY SELECTIVE ESTER HYDROLASE FROM PSEUDOMONAS SP - AN ATTRACTIVE ALTERNATIVE TO ESTER HYDROLYSIS
LAUMEN, K
BREITGOFF, D
SCHNEIDER, MP
[J]. JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS, 1988, (22) : 1459 - 1461
[10] Laumen K. E, 1987, THESIS BERGISCHE U W

← 1 2 →