GAS CHROMATOGRAPHIC DETERMINATION OF STARCH HYDROLYZATE SACCHARIDE DISTRIBUTION THROUGH MALTOHEPTAOSE

被引：17

作者：

BEADLE, JB

机构：

[1] Moffett Technical Center, CPC International, Argo, Ill. 60501

来源：

JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY | 1969年 / 17卷 / 04期

关键词：

D O I：

10.1021/jf60164a010

中图分类号：

S [农业科学];

学科分类号：

09 ;

摘要：

Through the use of short, lightly-loaded columns, the trimethylsilyl ethers of maltooligosaccharides up to the octaose can be eluted. The procedure describes a method for analyzing starch hydrolyzates through maltoheptaose with an accuracy equal to or better than that obtained by paper chromatography. Maltooctaose is severely absorbed on the column which prevents quantitative determination of this component. Over-all analytical time including sample preparation is less than 1 hour. © 1969, American Chemical Society. All rights reserved.

引用

页码：904 / &

共 8 条

[1] ALBERSHEIM PETER, 1967, CARBOHYD RES, V5, P340, DOI 10.1016/S0008-6215(00)80510-8
[2] GAS CHROMATOGRAPHY OF SUGARS AND OTHER POLYHYDROXY COMPOUNDS
BENTLEY, R
WELLS, WW
MAKITA, M
SWEELEY, CC
[J]. BIOCHEMICAL AND BIOPHYSICAL RESEARCH COMMUNICATIONS, 1963, 11 (01) : 14 - &
[3] BROBST KM, 1966, CEREAL CHEM, V43, P35
[4] BROBST KM, 1966, AM SOC BREW CHEM P, P71
[5] BROBST KM, 1967, 154 M ACS CHIC
[6] OTTER G E, 1967, Journal of the Institute of Brewing, V73, P570
[7] QUANTITATIVE DETERMINATION OF MONOSACCHARIDES AS THEIR ALDITOL ACETATES BY GAS LIQUID CHROMATOGRAPHY
SAWARDEKER, JS
SLONEKER, JH
JEANES, A
[J]. ANALYTICAL CHEMISTRY, 1965, 37 (12) : 1602 - +
[8] GAS-LIQUID CHROMATOGRAPHY OF TRIMETHYLSILYL DERIVATIVES OF SUGARS AND RELATED SUBSTANCES
SWEELEY, CC
BENTLEY, R
MAKITA, M
WELLS, WW
[J]. JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1963, 85 (16) : 2497 - &

← 1 →