MICROLASER ABLATION-INDUCTIVELY COUPLED PLASMA-MASS SPECTROMETRY .1. INSTRUMENTATION AND PERFORMANCE OF MICROLASER ABLATION SYSTEM

被引：33

作者：

HUANG, Y ^{[1
]}

SHIBATA, Y ^{[1
]}

MORITA, M ^{[1
]}

机构：

[1] NATL INST ENVIRONM STUDIES,PO 16-2 ONOGAWA,YATABE,IBARAKI 305,JAPAN

来源：

ANALYTICAL CHEMISTRY | 1993年 / 65卷 / 21期

关键词：

D O I：

10.1021/ac00069a011

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

A micro laser ablation system for the elemental analysis of a small area down to several microns in diameter was constructed, and its performance was investigated in combination with an inductively coupled plasma (ICP) mass spectrometry technique. A Q-switched, low-power Nd-YAG laser was used to ablate the samples. The products formed by laser ablation processes were trapped on a filter and then examined by scanning electron microscope. Entrainment and transport of ablated particulates were evaluated experimentally, and the detection limits for elements in an alloy sample were determined.

引用

页码：2999 / 3003

页数：5

共 23 条

[1] LASER VAPORIZATION OF SOLID METAL SAMPLES INTO AN INDUCTIVELY COUPLED PLASMA [J].

CARR, JW ;

HORLICK, G .

SPECTROCHIMICA ACTA PART B-ATOMIC SPECTROSCOPY, 1982, 37 (01) :1-15

[2] LASER SOLID SAMPLING FOR INDUCTIVELY COUPLED PLASMA MASS-SPECTROMETRY [J].

DENOYER, ER ;

FREDEEN, KJ ;

HAGER, JW .

ANALYTICAL CHEMISTRY, 1991, 63 (08) :A445-&

[3]

DITTRICH K, 1984, PROG ANAL ATOM SPECT, V7, P139

[4] DIRECT ATOMIC SPECTROMETRIC ANALYSIS BY SLURRY ATOMIZATION .7. ANALYSIS OF COAL USING INDUCTIVELY COUPLED PLASMA MASS-SPECTROMETRY [J].

EBDON, L ;

FOULKES, ME ;

PARRY, HGM ;

TYE, CT .

JOURNAL OF ANALYTICAL ATOMIC SPECTROMETRY, 1988, 3 (06) :753-761

[5] DIRECT ATOMIC SPECTROMETRIC ANALYSIS BY SLURRY ATOMIZATION .9. FUNDAMENTAL-STUDIES OF REFRACTORY SAMPLES [J].

EBDON, L ;

FOULKES, ME ;

HILL, S .

JOURNAL OF ANALYTICAL ATOMIC SPECTROMETRY, 1990, 5 (01) :67-73

[6] FUNDAMENTAL-STUDIES OF LASER ABLATION FOR THE INTRODUCTION OF POWDERED SOLID SAMPLES INTO AN INDUCTIVELY COUPLED PLASMA [J].

FURUTA, N .

APPLIED SPECTROSCOPY, 1991, 45 (08) :1372-1376

[7] SOLID SAMPLE INTRODUCTION BY LASER ABLATION FOR INDUCTIVELY COUPLED PLASMA SOURCE-MASS SPECTROMETRY [J].

GRAY, AL .

ANALYST, 1985, 110 (05) :551-556

[8] ATOMIC EMISSION-SPECTROMETRY OF SOLID SAMPLES WITH LASER VAPORIZATION MICROWAVE INDUCED PLASMA SYSTEM [J].

ISHIZUKA, T ;

UWAMINO, Y .

ANALYTICAL CHEMISTRY, 1980, 52 (01) :125-129

[9] INDUCTIVELY COUPLED PLASMA EMISSION-SPECTROMETRY OF SOLID SAMPLES BY LASER ABLATION [J].

ISHIZUKA, T ;

UWAMINO, Y .

SPECTROCHIMICA ACTA PART B-ATOMIC SPECTROSCOPY, 1983, 38 (03) :519-527

[10]

JACKSON SE, 1992, J CAN MINERAL, V30, P1049

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