SYNTHESIS AND STRUCTURES OF HOMOLEPTIC 2-METHYLPROPANE-2-THIOLATE COMPLEXES OF SAMARIUM AND YTTERBIUM

被引:43
作者
TATSUMI, K
AMEMIYA, T
KAWAGUCHI, H
TANI, K
机构
关键词
D O I
10.1039/c39930000773
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
The homoleptic 2-methylpropane-2-thiolate complexes [Li(tmeda)]3[Ln(SBut)6] (Ln = Yb 1 and Sm 2 have been synthesized and structurally characterized; 1 from the reaction of YbCl3 or YbI2(thf)x with LiSBut, and 2 from SmI2(thf)x and LiSBut, in the presence of N,N,N',N'-tetramethylethylenediamine (tmeda; thf = tetrahydrofuran).
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页码:773 / 774
页数:2
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