CONTROLLED CHEMICAL OXIDATION OF CARBON-FIBERS - AN XPS-XAES-SEM STUDY

被引:24
作者
DESIMONI, E
SALVI, AM
CASELLA, IG
DAMIANO, D
机构
[1] Dipartimento di Chimica, Universita Della Basilicata, Potenza, 85100
关键词
D O I
10.1002/sia.740201106
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
High-modulus, polyacrylonitrile-derived carbon fibres were chemically oxidized in concentrated sulphuric acid containing potassium permanganate. The pre- and post oxidation surface status of the fibres was characterized by x-ray photoelectron spectroscopy x-ray-excited Auger spectroscopy and scanning electron microscopy. Tests were made to evaluate the effects of temperature, time of treatment and permanganate concentration. The overall results are discussed in terms of flexibility and easiness of the treatment and of reproducibility of the chemical composition of the oxidized fibre surface.
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页码:909 / 918
页数:10
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