SYNTHESIS OF D TRANSITION-METAL SULFIDES FROM AMORPHOUS DITHIOOXAMIDE COMPLEXES

被引:47
作者
ABBOUDI, M [1 ]
MOSSET, A [1 ]
机构
[1] CEMES LOE,29 RUE J MARVIG,F-31055 TOULOUSE,FRANCE
关键词
D O I
10.1006/jssc.1994.1073
中图分类号
O61 [无机化学];
学科分类号
070301 ; 081704 ;
摘要
Sulfides of six transition or post-transition metals have been prepared by decomposition of amorphous dithiooxamide complexes. The best procedure of pyrolysis corresponds to a heating at 680°C under a dynamic vacuum during 4 hr. This preparation, without any added sulfurizing atmosphere, leads to carbon-free sulfides. © 1994 Academic Press, Inc.
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页码:70 / 73
页数:4
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