THE SYNTHESIS AND LOW-TEMPERATURE SINGLE-CRYSTAL X-RAY STRUCTURE OF THE CHARGE-TRANSFER COMPLEX ([9]ANES3)2(I2)4 ([9]ANES3=1,4,7-TRITHIACYCLONONANE)

被引:31
作者
BLAKE, AJ [1 ]
GOULD, RO [1 ]
RADEK, C [1 ]
SCHRODER, M [1 ]
机构
[1] UNIV EDINBURGH,DEPT CHEM,W MAINS RD,EDINBURGH EH9 3JJ,MIDLOTHIAN,SCOTLAND
关键词
D O I
10.1039/c39930001191
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Reaction of [9]aneS3(1,4,7-trithiacyclononane)and I2 in cold CH2Cl2 results in the formation of 1 : 1 and 1 : 2 adducts; the single crystal X-ray structure of the 1 : 2 adduct ([9]aneS3)2(I2)4 shows an unusual polymeric structure with I2 bridging [9]aneS3 thioether units.
引用
收藏
页码:1191 / 1193
页数:3
相关论文
共 21 条
[21]   SYNTHESIS AND CRYSTALLOGRAPHIC STUDIES OF CROWN THIOETHER COMPLEXES OF BISMUTH(III) [J].
WILLEY, GR ;
LAKIN, MT ;
ALCOCK, NW .
JOURNAL OF THE CHEMICAL SOCIETY-DALTON TRANSACTIONS, 1992, (04) :591-596