DETERMINATION OF TRIAZINE-HERBICIDES IN DRINKING-WATER BY A HPLC COLUMN-SWITCHING TECHNIQUE

被引：22

作者：

LINTELMANN, J ^{[1
]}

MENGEL, C ^{[1
]}

KETTRUP, A ^{[1
]}

机构：

[1] GESELL STRAHLEN & UMWELTFORSCH MBH,FORSCHUNGSZENTRUM,INST OKOL CHEM,INGOLSTADTER LANDSTR 1,W-8042 NEUHERBERG,GERMANY

来源：

FRESENIUS JOURNAL OF ANALYTICAL CHEMISTRY | 1993年 / 346卷 / 6-9期

关键词：

D O I：

10.1007/BF00321285

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

A semi-automatic coupled-column HPLC-method for the rapid determination of desethylatrazine, simazine, atrazine and terbuthylazine in drinking water was developed. Tenax TA was used as precolumn packing material. 100 ml of the water sample are percolated through the precolumn, on which the analytes are preconcentrated and prefractionated. After the HPLC-integrated sample processing the triazines are transferred to the series-connected analytical column, where separation and detection takes place. The method leads to detection limits between 15 and 32 ng/l. The recovery rates range from 46 to 96% in drinking water.

引用

页码：752 / 756

页数：5

共 32 条

[21] HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY MASS-SPECTROMETRY OF TRIAZINE HERBICIDES [J].

PARKER, CE ;

HANEY, CA ;

HARVAN, DJ ;

HASS, JR .

JOURNAL OF CHROMATOGRAPHY, 1982, 242 (01) :77-96

[22] DETERMINATION OF TRIAZINES IN WATER BY GC AND LC [J].

POPL, M ;

VOZNAKOVA, Z ;

TATAR, V ;

STRNADOVA, J .

JOURNAL OF CHROMATOGRAPHIC SCIENCE, 1983, 21 (01) :39-42

[23] HIGH-PRESSURE LIQUID-CHROMATOGRAPHIC DETERMINATION OF HYDROXY-S-TRIAZINE RESIDUES IN PLANT-MATERIAL [J].

RAMSTEINER, KA ;

HORMANN, WD .

JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 1979, 27 (05) :934-938

[24] DETERMINATION OF NITROGEN-CONTAINING PESTICIDES BY HPLC WITH DIODE-ARRAY DETECTION [J].

REUPERT, R ;

PLOGER, E .

FRESENIUS ZEITSCHRIFT FUR ANALYTISCHE CHEMIE, 1988, 331 (05) :503-509

[25]

Reupert R, 1989, VOM WASSER, V72, P211

[26] MULTI-RESIDUE-ANALYSIS OF PESTICIDES BY HPLC AFTER SOLID-PHASE EXTRACTION [J].

SCHLETT, C .

FRESENIUS JOURNAL OF ANALYTICAL CHEMISTRY, 1991, 339 (06) :344-347

[27] SOLID-PHASE EXTRACTION OF HERBICIDES FROM WELL WATER FOR DETERMINATION BY GAS-CHROMATOGRAPHY MASS-SPECTROMETRY [J].

SCHUETTE, SA ;

SMITH, RG ;

HOLDEN, LR ;

GRAHAM, JA .

ANALYTICA CHIMICA ACTA, 1990, 236 (01) :141-144

[28] RECOVERY OF ORGANIC-COMPOUNDS FROM LARGE-VOLUME AQUEOUS SAMPLES USING ONLINE LIQUID-CHROMATOGRAPHIC PRECONCENTRATION TECHNIQUES [J].

SUBRA, P ;

HENNION, MC ;

ROSSET, R ;

FREI, RW .

JOURNAL OF CHROMATOGRAPHY, 1988, 456 (01) :121-141

[29] HIGH-RESOLUTION GAS-CHROMATOGRAPHIC DETERMINATION OF NITROGEN AND PHOSPHORUS-COMPOUNDS IN COMPLEX ORGANIC MIXTURES BY A TUNABLE SELECTIVE THERMIONIC DETECTOR [J].

VERGA, GR .

JOURNAL OF CHROMATOGRAPHY, 1983, 279 (NOV) :657-665

[30] REVERSED-PHASE SOLID-PHASE EXTRACTION FOR AQUEOUS ENVIRONMENTAL SAMPLE PREPARATION IN HERBICIDE RESIDUE ANALYSIS [J].

WELLS, MJM ;

MICHAEL, JL .

JOURNAL OF CHROMATOGRAPHIC SCIENCE, 1987, 25 (08) :345-350

← 1 2 3 4 →