USE OF NEW SILYLATING AGENTS FOR SEPARATION AND IDENTIFICATION OF PROSTAGLANDINS BY GAS-CHROMATOGRAPHY AND GAS CHROMATOGRAPHY-MASS SPECTROMETRY

被引：21

作者：

MIYAZAKI, H ^{[1
]}

ISHIBASHI, M ^{[1
]}

YAMASHITA, K ^{[1
]}

KATORI, M ^{[1
]}

机构：

[1] KITAZATO UNIV,SCH MED,DEPT PHARMACOL,SAGAMIHARA,KANAGAWA 228,JAPAN

来源：

JOURNAL OF CHROMATOGRAPHY | 1978年 / 153卷 / 01期

关键词：

D O I：

10.1016/S0021-9673(00)89858-1

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

引用

页码：83 / 90

页数：8

共 14 条

[1]

Crain P F, 1975, Methods Enzymol, V35, P359, DOI 10.1016/0076-6879(75)35176-8

[2] GAS CHROMATOGRAPHY-MASS SPECTROMETRY OF O-METHYLOXIME DERIVATIVES OF PROSTAGLANDINS [J].

GREEN, K .

CHEMISTRY AND PHYSICS OF LIPIDS, 1969, 3 (03) :254-&

[3] METHODS FOR QUANTITATIVE-ANALYSIS OF PGF2-ALPHA, PGE2, 9-ALPHA, 11-ALPHA-DIHYDROXY-15-KETO-PROST-5-ENOIC ACID AND 9-ALPHA, 11-ALPHA, 15-TRIHYDROXY-PROST-5-ENOIC ACID FROM BODY-FLUIDS USING DEUTERATED CARRIERS AND GAS CHROMATOGRAPHY MASS SPECTROMETRY [J].

GREEN, K ;

GRANSTRO.E ;

SAMUELSS.B ;

AXEN, U .

ANALYTICAL BIOCHEMISTRY, 1973, 54 (02) :434-453

[4]

Gutierrez-Cernosek R M, 1975, Methods Enzymol, V35, P287, DOI 10.1016/0076-6879(75)35166-5

[5]

Jouvenaz G H, 1970, Biochim Biophys Acta, V202, P231, DOI 10.1016/0005-2760(70)90246-8

[6] GAS-CHROMATOGRAPHIC DETERMINATION OF NANOGRAM AMOUNTS OF PROSTAGLANDINS-E AND F [J].

JOUVENAZ, GH ;

NUGTEREN, DH ;

VANDORP, DA .

PROSTAGLANDINS, 1973, 3 (02) :175-187

[7] GAS-CHROMATOGRAPHY OF PROSTAGLANDIN HEPTAFLUOROBUTYRATE METHYL-ESTERS [J].

MIDDLEDITCH, BS ;

DESIDERIO, DM .

PROSTAGLANDINS, 1972, 2 (03) :195-+

[8] USE OF SILYLATING AGENTS FOR IDENTIFICATION OF HYDROXYLATED STEROIDS BY GAS-CHROMATOGRAPHY AND GAS CHROMATOGRAPHY MASS SPECTROMETRY - DISCRIMINATION BETWEEN PHENOLIC AND ALCOHOLIC HYDROXYL-GROUPS [J].

MIYAZAKI, H ;

ISHIBASHI, M ;

ITOH, M ;

YAMASHITA, K ;

NAMBARA, T .

JOURNAL OF CHROMATOGRAPHY, 1977, 133 (02) :311-318

[9] USE OF NEW SILYLATING AGENTS FOR IDENTIFICATION OF HYDROXYLATED STEROIDS BY GAS-CHROMATOGRAPHY AND GAS-CHROMATOGRAPHY MASS-SPECTROMETRY [J].

MIYAZAKI, H ;

ISHIBASHI, M ;

ITOH, M ;

NAMBARA, T .

BIOMEDICAL MASS SPECTROMETRY, 1977, 4 (01) :23-35

[10]

MIYAZAKI H, 1977, 97TH ANN M PHARM SOC

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