FLOW-THROUGH, MICROWAVE-HEATED DIGESTION CHAMBER FOR AUTOMATED SAMPLE PREPARATION PRIOR TO INDUCTIVELY-COUPLED PLASMA SPECTROCHEMICAL ANALYSIS

被引：14

作者：

STEWART, LJM ^{[1
]}

BARNES, RM ^{[1
]}

机构：

[1] UNIV MASSACHUSETTS,LEDERLE GRAD RES CTR,DEPT CHEM,AMHERST,MA 01003

来源：

ANALYST | 1994年 / 119卷 / 05期

关键词：

SAMPLE PREPARATION; MICROWAVE DIGESTION; FLOW-THROUGH DEVICE; BIOLOGICAL MATERIAL; METAL DETERMINATION; INDUCTIVELY COUPLED PLASMA ATOMIC EMISSION SPECTROMETRY;

D O I：

10.1039/an9941901003

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

A microwave-heated, flow-through digestion device was designed for a commercial, focused microwave system and applied to the on-line preparation of biological samples including milk, whole blood and urine. Accurate and precise results were obtained by inductively coupled plasma atomic emission spectrometry with solutions prepared by on-line stopped-flow digestion.

引用

页码：1003 / 1010

页数：8

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