DIRECT ANALYSIS OF SOLID SAMPLE WITH ULTRAFINE PARTICLE GENERATION INDUCTIVELY COUPLED PLASMA EMISSION-SPECTROSCOPY

被引:22
作者
ONO, A [1 ]
SAEKI, M [1 ]
CHIBA, K [1 ]
机构
[1] NIPPON STEEL CORP,ANAL RES LAB,1618 IDA,NAKAHARA KU,KAWASAKI 211,JAPAN
关键词
ELECTRIC SPARKS - PLASMAS - Applications - SPECTROSCOPY; EMISSION; -; Applications;
D O I
10.1366/0003702874447941
中图分类号
TH7 [仪器、仪表];
学科分类号
0804 ; 080401 ; 081102 ;
摘要
An ultrafine particle generation (UFP) system has been developed for the direct analysis of solid metal samples by inductively coupled plasma (ICP) emission spectrometry. In this system fine particles are generated from solid samples with the use of a spark discharge and then swept into the ICP. The spark discharge conditions involving the electrode gap and the analytical performance of the ICP system are investigated. Analytical calibration curves are presented for steel samples. The NBS standard reference materials are analyzed by the proposed system.
引用
收藏
页码:970 / 976
页数:7
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