SI-29 CROSS-POLARIZATION MAGIC ANGLE SPINNING NMR EVIDENCE FOR GEMINAL SILANOLS ON VACUUM-ACTIVATED AEROSIL SILICA

被引：70

作者：

MORROW, BA ^{[1
]}

GAY, ID ^{[1
]}

机构：

[1] SIMON FRASER UNIV,DEPT CHEM,BURNABY V5A 1S6,BC,CANADA

来源：

JOURNAL OF PHYSICAL CHEMISTRY | 1988年 / 92卷 / 20期

关键词：

D O I：

10.1021/j100331a008

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

引用

页码：5569 / 5571

页数：3

共 30 条

[1] SOL-GEL TRANSITION IN SIMPLE SILICATES .3. STRUCTURAL STUDIES DURING DENSIFICATION [J].

BRINKER, CJ ;

TALLANT, DR ;

ROTH, EP ;

ASHLEY, CS .

JOURNAL OF NON-CRYSTALLINE SOLIDS, 1986, 82 (1-3) :117-126

[2] NMR CONFIRMATION OF STRAINED DEFECTS IN AMORPHOUS SILICA [J].

BRINKER, CJ ;

KIRKPATRICK, RJ ;

TALLANT, DR ;

BUNKER, BC ;

MONTEZ, B .

JOURNAL OF NON-CRYSTALLINE SOLIDS, 1988, 99 (2-3) :418-428

[3] QUANTITATIVELY RELIABLE SI-29 MAGIC-ANGLE SPINNING NUCLEAR MAGNETIC-RESONANCE SPECTRA OF SURFACES AND SURFACE-IMMOBILIZED SPECIES AT HIGH-FIELD USING A CONVENTIONAL HIGH-RESOLUTION SPECTROMETER [J].

FYFE, CA ;

GOBBI, GC ;

KENNEDY, GJ .

JOURNAL OF PHYSICAL CHEMISTRY, 1985, 89 (02) :277-281

[4] A MAGIC-ANGLE SPINNER FOR VACUUM-SEALED SAMPLES [J].

GAY, ID .

JOURNAL OF MAGNETIC RESONANCE, 1984, 58 (03) :413-420

[5] INFRARED STUDY OF LOW-TEMPERATURE ADSORPTION .1. CO ON AEROSIL - INTERPRETATION OF THE HYDRATED SILICA SPECTRUM [J].

GHIOTTI, G ;

GARRONE, E ;

MORTERRA, C ;

BOCCUZZI, F .

JOURNAL OF PHYSICAL CHEMISTRY, 1979, 83 (22) :2863-2869

[6] SI-29-MAS-NMR INVESTIGATION ON SILICA GLASS PREPARED BY THE DRYING CONTROL CHEMICAL ADDITIVES METHOD [J].

GRIMMER, AR ;

ROSENBERGER, H ;

BURGER, H ;

VOGEL, W .

JOURNAL OF NON-CRYSTALLINE SOLIDS, 1988, 99 (2-3) :371-378

[7] REACTIONS OF CHLOROSILANES WITH SILICA SURFACES [J].

HAIR, ML ;

HERTL, W .

JOURNAL OF PHYSICAL CHEMISTRY, 1969, 73 (07) :2372-&

[8]

Harris R. K., 1978, NMR PERIODIC TABLE

[9] REACTION OF SILICA SURFACES WITH HYDROGEN SEQUESTERING AGENTS [J].

HOCKEY, JA .

JOURNAL OF PHYSICAL CHEMISTRY, 1970, 74 (12) :2570-&

[10] NOVEL ASPECTS OF MID AND FAR IR FOURIER SPECTROSCOPY APPLIED TO SURFACE AND ADSORPTION STUDIES ON SIO2 [J].

HOFFMANN, P ;

KNOZINGER, E .

SURFACE SCIENCE, 1987, 188 (1-2) :181-198

← 1 2 3 →