CRYSTAL-STRUCTURE OF 2-TRIPHENYLSTANNYL 1,2-BENZISOTHIAZOL-3(2H)-ONE 1,1-DIOXIDE-QUINOLINE N-OXIDE (1/1) MOLECULAR-COMPLEX

被引：7

作者：

NG, SW

机构：

[1] University of Malaya, Institute of Advanced Studies

来源：

ZEITSCHRIFT FUR KRISTALLOGRAPHIE | 1994年 / 209卷 / 10期

关键词：

CRYSTAL STRUCTURE;

D O I：

10.1524/zkri.1994.209.10.813

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

The coordination environment of the tin atom in 2-triphenylstannyl 1,2-benzisothiazol-3(2H)-one 1,1-dioxide . quinoline N-oxide, C34H26N2O3SSn, is a trigonal bipyramid in which the ipso-carbons of the phenyl rings (Sn - C = 2.117(9) angstrom, 2.122(9) angstrom, 2.128(9) angstrom; SIGMA C - Sn - C = 359.9(9)-degrees) comprise the equatorial, and the imido nitrogen of the 1,2-benzoisothiazol-3(2H)-onyl 1,1-dioxide anion (Sn - N = 2.266(7) angstrom) and the oxygen of quinoline N-oxide donor (Sn <-- O = 2.319(6) angstrom) the apical (O - Sn <-- O = 175.4(2)degrees) sites.

引用

页码：813 / 815

页数：3

共 13 条

[1]

[Anonymous], 1974, INT TABLES XRAY CRYS, VIV

[2]

DAS VGK, 1986, J ORGANOMET CHEM, V311, P289

[3]

JOHNSON CK, 1976, ORTEP 2 FORTRAN THER

[4]

KILLEAN RCG, 1969, ACTA CRYSTALLOGR B, V25, P1650