SEPARATION OF C-60 AND C-70 ON POLYSTYRENE GEL WITH TOLUENE AS MOBILE PHASE

被引:33
作者
GUGEL, A [1 ]
MULLEN, K [1 ]
机构
[1] MAX PLANCK INST POLYMER RES,ACKERMANNWEG 10,W-6500 MAINZ,GERMANY
来源
JOURNAL OF CHROMATOGRAPHY | 1993年 / 628卷 / 01期
关键词
D O I
10.1016/0021-9673(93)80328-6
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
The separation of C60 and C70 on polystyrene gel using toluene as mobile phase is described. A fully automated system was designed that permits the separation of 5-10 g of C60-C70 mixture within 24 h on a column of only 20 mm I.D. The purity of the isolated C60 is greater than that achieved by standard procedures (separation on alumina) and the recovery is nearly 100%.
引用
收藏
页码:23 / 29
页数:7
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