BENZOQUINOLIZINE AND INDOLOQUINOLIZINE DERIVATIVES .17. SYNTHESIS OF THE 1,2,3,4A,6,7,8,9,13B-DECAHYDRO-9AH-PYRIDO[1,2-F]PHENANTRIDINE ISOMERS

被引：3

作者：

LAUS, G ^{[1
]}

VANBINST, G ^{[1
]}

机构：

[1] VRIJE UNIV BRUSSEL,ORGAN CHEM LAB,B-1050 BRUSSELS,BELGIUM

来源：

TETRAHEDRON | 1979年 / 35卷 / 07期

关键词：

D O I：

10.1016/0040-4020(79)80105-2

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

The four possible diastereoisomers of 1,2,3,4a,6,7,8,9,13b - decahydro - 9aH- pyrido[1,2 - f]phenantridine were obtained by reduction of the enamine 1,2,3,4,6,7,8,9 - octahydro - 9aH - pyrido[1,2 - f]phenantridine or of its corresponding iminiumsalt. We report also the synthesis of two isomers of the title compound starting from trans-2-phenyl-cyclohexylamine. © 1979.

引用

页码：849 / 855

页数：7

共 25 条

[1]

BARTLETT PD, 1940, J AM CHEM SOC, P2936

[2]

Brown, 1972, BORANES ORGANIC CHEM

[3] SELECTIVE REDUCTIONS .3. FURTHER STUDIES OF REACTION OF ALCOHOLS WITH LITHIUM ALUMINUM HYDRIDE AS ROUTE TO LITHIUM ALKOXYALUMINOHYDRIDES [J].

BROWN, HC ;

SHOAF, CJ .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1964, 86 (06) :1079-&

[4] LITHIUM TRI-SEC-BUTYLBOROHYDRIDE - NEW REAGENT FOR REDUCTION OF CYCLIC AND BICYCLIC KETONES WITH SUPER STEREOSELECTIVITY - REMARKABLY SIMPLE AND PRACTICAL PROCEDURE FOR CONVERSION OF KETONES TO ALCOHOLS IN EXCEPTIONALLY HIGH STEREOCHEMICAL PURITY [J].

BROWN, HC ;

KRISHNAMURTHY, S .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1972, 94 (20) :7159-+

[5]

Eliel E. E, 1961, REC CHEM PROGR, V22, P129

[6]

EVANS JCW, 1943, ORG SYNTH, V2, P517

[7]

HORII ZI, 1968, CHEM PHARM BULL, V16, P1472

[8]

Horiuti J., 1934, T FARADAY SOC, V30, P1164, DOI DOI 10.1039/TF9343001164

[9] RACEMISATION .I. RACEMISATION OF PROTOBERBERINES UNDER CONDITIONS OF CATALYTIC HYDROGENATION [J].

KAMETANI, T ;

IHARA, M .

JOURNAL OF THE CHEMICAL SOCIETY C-ORGANIC, 1968, (02) :191-&

[10] HYDROBORATION AND REDUCTION OF ENAMINES .3. REACTION OF EXO-ENAMINES AND ENDO-ENAMINES WITH DIBORANE AND SODIUM-BOROHYDRIDE [J].

KUDO, T ;

NOSE, A .

YAKUGAKU ZASSHI-JOURNAL OF THE PHARMACEUTICAL SOCIETY OF JAPAN, 1974, 94 (11) :1475-1483

← 1 2 3 →