APPLICATIONS OF THE IMPROVED COMPUTERIZED ANALYSIS OF 2D INADEQUATE SPECTRA

被引：28

作者：

DUNKEL, R

MAYNE, CL

FOSTER, MP

IRELAND, CM

LI, D

OWEN, NL

PUGMIRE, RJ

GRANT, DM

机构：

[1] UNIV UTAH,DEPT CHEM,SALT LAKE CITY,UT 84112

[2] UNIV UTAH,DEPT MED CHEM,SALT LAKE CITY,UT 84112

[3] UNIV UTAH,DEPT FUELS ENGN,SALT LAKE CITY,UT 84112

[4] BRIGHAM YOUNG UNIV,DEPT CHEM,PROVO,UT 84602

来源：

ANALYTICAL CHEMISTRY | 1992年 / 64卷 / 24期

关键词：

D O I：

10.1021/ac00048a012

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

This paper illustrates the use of the program CCBOND to determine the carbon skeletons of bioorganic molecules in low concentration samples. Discussed is the structure elucidation of bistramide A, a compound extracted from a Fijian Lissoclinum sp. and cholesterol in 71- and 20-mumol samples, respectively. The detection limit of the automated bond extraction is shown to be dramatically improved compared to the manual interpretation of 20 INADEOUATE spectra.

引用

页码：3150 / 3160

页数：11

共 23 条

[1] AN NMR TECHNIQUE FOR TRACING OUT THE CARBON SKELETON OF AN ORGANIC-MOLECULE
BAX, A
FREEMAN, R
FRENKIEL, TA
[J]. JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1981, 103 (08) : 2102 - 2104
[2] NATURAL ABUNDANCE C-13-C-13 COUPLING OBSERVED VIA DOUBLE-QUANTUM COHERENCE
BAX, A
FREEMAN, R
KEMPSELL, SP
[J]. JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1980, 102 (14) : 4849 - 4851
[3] INVESTIGATION OF C-13-C-13 COUPLINGS IN NATURAL ABUNDANCE SAMPLES - THE STRONG COUPLING CASE
BAX, A
FREEMAN, R
[J]. JOURNAL OF MAGNETIC RESONANCE, 1980, 41 (03) : 507 - 511
[4] C-13 NMR-STUDIES .69. C-13 NMR-SPECTRA OF STEROIDS - SURVEY AND COMMENTARY
BLUNT, JW
STOTHERS, JB
[J]. ORGANIC MAGNETIC RESONANCE, 1977, 9 (08): : 439 - 464
[5] STRUCTURE GENERATION BY REDUCTION - A NEW STRATEGY FOR COMPUTER-ASSISTED STRUCTURE ELUCIDATION
CHRISTIE, BD
MUNK, ME
[J]. JOURNAL OF CHEMICAL INFORMATION AND COMPUTER SCIENCES, 1988, 28 (02): : 87 - 93
[6] THE APPLICATION OF TWO-DIMENSIONAL NUCLEAR MAGNETIC-RESONANCE SPECTROSCOPY IN COMPUTER-ASSISTED STRUCTURE ELUCIDATION
CHRISTIE, BD
MUNK, ME
[J]. ANALYTICA CHIMICA ACTA, 1987, 200 (01) : 347 - 361
[7] NOVEL CYTO-TOXIC COMPOUNDS FROM THE ASCIDIAN LISSOCLINUM-BISTRATUM
DEGNAN, BM
HAWKINS, CJ
LAVIN, MF
MCCAFFREY, EJ
PARRY, DL
WATTERS, DJ
[J]. JOURNAL OF MEDICINAL CHEMISTRY, 1989, 32 (06) : 1354 - 1359
[8] COMPUTERIZED ANALYSIS OF 2D INADEQUATE SPECTRA
DUNKEL, R
MAYNE, CL
CURTIS, J
PUGMIRE, RJ
GRANT, DM
[J]. JOURNAL OF MAGNETIC RESONANCE, 1990, 90 (02) : 290 - 302
[9] IMPROVEMENTS IN THE COMPUTERIZED ANALYSIS OF 2D INADEQUATE SPECTRA
DUNKEL, R
MAYNE, CL
PUGMIRE, RJ
GRANT, DM
[J]. ANALYTICAL CHEMISTRY, 1992, 64 (24) : 3133 - 3149
[10] DUNKEL R, 1990, THESIS U UTAH

← 1 2 3 →