APPLICATIONS OF THE IMPROVED COMPUTERIZED ANALYSIS OF 2D INADEQUATE SPECTRA

被引：28

作者：

DUNKEL, R

MAYNE, CL

FOSTER, MP

IRELAND, CM

LI, D

OWEN, NL

PUGMIRE, RJ

GRANT, DM

机构：

[1] UNIV UTAH,DEPT CHEM,SALT LAKE CITY,UT 84112

[2] UNIV UTAH,DEPT MED CHEM,SALT LAKE CITY,UT 84112

[3] UNIV UTAH,DEPT FUELS ENGN,SALT LAKE CITY,UT 84112

[4] BRIGHAM YOUNG UNIV,DEPT CHEM,PROVO,UT 84602

来源：

ANALYTICAL CHEMISTRY | 1992年 / 64卷 / 24期

关键词：

D O I：

10.1021/ac00048a012

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

This paper illustrates the use of the program CCBOND to determine the carbon skeletons of bioorganic molecules in low concentration samples. Discussed is the structure elucidation of bistramide A, a compound extracted from a Fijian Lissoclinum sp. and cholesterol in 71- and 20-mumol samples, respectively. The detection limit of the automated bond extraction is shown to be dramatically improved compared to the manual interpretation of 20 INADEOUATE spectra.

引用

页码：3150 / 3160

页数：11