HIGH-TEMPERATURE NMR USING INDUCTIVE HEATING

被引：17

作者：

MARESCH, GG ^{[1
]}

KENDRICK, RD ^{[1
]}

YANNONI, CS ^{[1
]}

机构：

[1] IBM CORP,ALMADEN RES CTR,DIV RES,SAN JOSE,CA 95120

来源：

REVIEW OF SCIENTIFIC INSTRUMENTS | 1990年 / 61卷 / 01期

关键词：

D O I：

10.1063/1.1141903

中图分类号：

TH7 [仪器、仪表];

学科分类号：

0804 ; 080401 ; 081102 ;

摘要：

We report a simple, efficient method for carrying out nuclear magnetic resonance (NMR) experiments at high temperature in any NMR probe without modification. The sample tube is coated with a thin film of metal and the rf coil used for the NMR experiment is used to inductively heat the film, thus heating the sample inside the tube. Using this approach, we have obtained both proton and high-resolution carbon-13 NMR spectra at temperatures as high as 730 K.

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页码：77 / 80

页数：4

相关论文

共 21 条

[11]

MARESCH GG, UNPUB

[12] HIGH-TEMPERATURE AND HIGH-FIELD NUCLEAR MAGNETIC-RESONANCE INSTRUMENT [J].

PLOUMBIDIS, D .

REVIEW OF SCIENTIFIC INSTRUMENTS, 1979, 50 (09) :1133-1135

[13] DEWAR SYSTEM TO ATTAIN-140 TO 550 DEGREESC IN NMR CROSSCOIL PROBE [J].

SCHREIBER, DS .

REVIEW OF SCIENTIFIC INSTRUMENTS, 1964, 35 (11) :1582-&

[14] HOMOGENEOUS VERY HIGH-TEMPERATURE MINIFURNACE [J].

SHAHAM, M ;

ELHANANY, U .

JOURNAL OF PHYSICS E-SCIENTIFIC INSTRUMENTS, 1979, 12 (05) :359-360

[15] HIGH-TEMPERATURE FURNACE FOR NMR MEASUREMENTS [J].

SOLLER, FX ;

SOTIER, S ;

COUFAL, H ;

HACKSTEIN, K .

JOURNAL OF PHYSICS E-SCIENTIFIC INSTRUMENTS, 1979, 12 (07) :577-579

[16] NEW PROBE FOR HIGH-TEMPERATURE NMR-SPECTROSCOPY WITH PPM RESOLUTION [J].

STEBBINS, JF ;

SCHNEIDER, E ;

MURDOCH, JB ;

PINES, A ;

CARMICHAEL, ISE .

REVIEW OF SCIENTIFIC INSTRUMENTS, 1986, 57 (01) :39-42

[17] FURNACE TO REACH 1100 DEGREESC IN NMR CROSSCOIL PROBES [J].

STYLES, GA ;

SHEFFIELD, TB .

JOURNAL OF PHYSICS E-SCIENTIFIC INSTRUMENTS, 1976, 9 (03) :223-225

[18] SIMPLE FURNACE FOR HIGH TEMPERATURE NUCLEAR MAGNETIC RESONANCE EXPERIMENTS [J].

WARREN, WW ;

CLARK, WG .

JOURNAL OF PHYSICS E-SCIENTIFIC INSTRUMENTS, 1968, 1 (10) :1019-&

[19]

WEBSTER DS, 1978, REV SCI INSTRUM, V50, P390

[20] USE OF FLUOROPTIC THERMOMETER TEMPERATURE SENSING FOR HIGH-RESOLUTION TEMPERATURE-CONTROLLED NMR APPLICATIONS [J].

WILLIAMS, HJ ;

GAO, YD ;

SCOTT, AI ;

GROSS, MH ;

SUN, MH .

JOURNAL OF MAGNETIC RESONANCE, 1988, 78 (02) :338-343