SYNTHESIS OF MICROCRYSTALLINE TITANIA IN ORGANIC MEDIA

被引:20
作者
INOUE, M
KOMINAMI, H
OTSU, H
INUI, T
机构
[1] Department of Hydrocarbon Chemistry, Faculty of Engineering, Kyoto University, Yoshida
关键词
D O I
10.1246/nikkashi.1991.1364
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Reaction of oxobis(2, 4-pentanedionato-O, O')titanium (TiO(acac)2) or titanium isopropoxide (TIP) in various organic media was examined and found to afford microcrystalline anatase. The product having the smallest crystallite size and the largest surface area was obtained by the reaction of TiO(acac)2 in toluene at 250-degrees-C. The product preserved relatively high surface area even after calcination at 550-degrees-C in an air flow.
引用
收藏
页码:1364 / 1366
页数:3
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