STUDY OF THE STABILITY OF EXTRACTABLE TRACE-METAL CONTENTS IN A RIVER SEDIMENT USING SEQUENTIAL EXTRACTION

被引:65
作者
FIEDLER, HD
LOPEZSANCHEZ, JF
RUBIO, R
RAURET, G
QUEVAUVILLER, P
URE, AM
MUNTAU, H
机构
[1] COMMISS EUROPEAN COMMUNITIES,COMMUNITY BUR REFERENCE,DIRECTORATE GEN SCI RES & DEV,B-1049 BRUSSELS,BELGIUM
[2] UNIV STRATHCLYDE,DEPT PURE & APPL CHEM,GLASGOW G1 1XL,SCOTLAND
[3] COMMISS EUROPEAN COMMUNITIES,JOINT RES CTR,INST ENVIRONM,I-21020 ISPRA,ITALY
关键词
SEQUENTIAL EXTRACTION SCHEME; EXTRACTABLE TRACE METAL CONTENT; SEDIMENT; HOMOGENEITY; STABILITY;
D O I
10.1039/an9941901109
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
Sequential extraction schemes have been used in recent years to study the environmental behaviour of trace metals present in soils and sediments. Owing to the variety of the different extraction procedures, the results obtained were not comparable as they were highly dependent on the procedure. Moreover, the lack of suitable reference materials for this type of analysis prevents quality control of the measurements. In 1987 the Community Bureau of Reference (BCR, now Measuring and Testing Programme) started a programme to harmonize the methodology and to produce certified reference materials. This paper presents the work carried out to prepare a river sediment sample to be analysed in an intercomparison exercise using a common sequential extraction scheme adopted at Sitges by a group of European experts. The studies of homogeneity and stability with time of the extractable trace metal contents in the sample are also reported.
引用
收藏
页码:1109 / 1114
页数:6
相关论文
共 13 条
[11]  
URE A, 1993, EUR14763 EN CEC REP
[12]  
1981, PHOTOMETRIC FLUOROME
[13]  
1993, INT J ENV ANAL CHEM, V51