SYNTHESIS OF C-14-LABELED FLAME RETARDANTS - C-14-LABELED-TETRABROMOPHTHALIC ANHYDRIDE AND TETRABROMOBISPHENOL-A

被引：13

作者：

SUSAN, AB

EBERT, DA

DUNCAN, WP

机构：

[1] Midwest Research Institute, Kansas City, Missouri, 64110

来源：

JOURNAL OF LABELLED COMPOUNDS & RADIOPHARMACEUTICALS | 1979年 / 16卷 / 04期

关键词：

Flame retardants; Phthalic‐1,2,3,4,5,6‐U‐[!sup]14[!/sup]C acid; Tetrabromobisphenol‐A‐([!sup]14[!/sup]C‐labeled); Tetrabromophthalic‐1,2,3,4,5,6‐U‐[!sup]14[!/sup]C anhydride;

D O I：

10.1002/jlcr.2580160410

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

The multistep syntheses of tetrabromophthalic‐1,2,3,4,5,6‐U‐14C anhydride 6, and 3,5,3′,5′‐tetrabromo‐4,4′‐isopropylidenedi‐(phenol‐U‐14C) 11, are described. The synthesis pathway to 6 includes a novel preparation of phthalic acid‐1,2,3,4,5,6‐U‐14C acid from benzene‐U‐14C. Both 6 and 11 were obtained in 9% overall radiochemical yield (based on benzene‐U‐14C). Copyright © 1979 John Wiley & Sons, Ltd.

引用

页码：579 / 589

页数：11