SIMULTANEOUS THERMOGRAVIMETRY DIFFERENTIAL THERMAL-ANALYSIS MASS-SPECTROMETRY (TG-DTA-MS) USING A HEATED CAPILLARY INTERFACE

被引：10

作者：

MCGHIE, AR

机构：

[1] Laboratory for Research on the Structure of Matter, University of Pennsylvania, Philadelphia

来源：

THERMOCHIMICA ACTA | 1994年 / 234卷

关键词：

D O I：

10.1016/0040-6031(94)85132-8

中图分类号：

O414.1 [热力学];

学科分类号：

摘要：

A quadrupole mass spectrometer (MS) has been successfully and simply coupled to a simultaneous thermogravimetric analyzer-differential thermal analyzer (TG-DTA) through a heated capillary interface. The system has been used to study both calcium oxalate monohydrate and to interpret the unusual vaporization behavior of Buckminsterfullerene C60 on heating in an inert atmosphere.

引用

页码：21 / 29

页数：9

共 8 条

[1]

CHARSLEY EL, 1990, AM LAB JAN, P21

[2] SOME APPLICATIONS OF THERMAL-ANALYSIS TO FULLERENES [J].

GALLAGHER, PK ;

ZHONG, Z .

JOURNAL OF THERMAL ANALYSIS, 1992, 38 (10) :2247-2255

[3] SOLID C-60 - A NEW FORM OF CARBON [J].

KRATSCHMER, W ;

LAMB, LD ;

FOSTIROPOULOS, K ;

HUFFMAN, DR .

NATURE, 1990, 347 (6291) :354-358

[4] C-60 - BUCKMINSTERFULLERENE [J].

KROTO, HW ;

HEATH, JR ;

OBRIEN, SC ;

CURL, RF ;

SMALLEY, RE .

NATURE, 1985, 318 (6042) :162-163

[5]

MCGHIE AR, IN PRESS

[6] HEATS OF SUBLIMATION FROM A POLYCRYSTALLINE MIXTURE OF C60 AND C70 [J].

PAN, C ;

SAMPSON, MP ;

CHAI, Y ;

HAUGE, RH ;

MARGRAVE, JL .

JOURNAL OF PHYSICAL CHEMISTRY, 1991, 95 (08) :2944-2946

[7]

VANTETS A, 1969, THERM ANAL, V1, P121

[8]

WIEDEMANN HG, 1964, CHEMIE ING TECHN, V36, P1105

← 1 →