SYNTHESIS OF 1,3,3-TRINITROAZETIDINE

被引：35

作者：

AXENROD, T ^{[1
]}

WATNICK, C ^{[1
]}

YAZDEKHASTI, H ^{[1
]}

DAVE, PR ^{[1
]}

机构：

[1] ARDEC,GEOCTR INC,LAKE HOPATCONG,NJ 07849

来源：

TETRAHEDRON LETTERS | 1993年 / 34卷 / 42期

关键词：

D O I：

10.1016/S0040-4039(00)61673-8

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

The 1-butyldimethylsilyl ether of 3-(p-toluenesulfonamido)propane-2-ol-1-(p-toluenesulfonate) on treatment with LiH undergoes ring closure to the corresponding azetidine which is readily converted to N-tosyl-3-azetidinone oxime. By oxidative nitrolysis the latter affords 1.3,3-trinitroazetidine.

引用

页码：6677 / 6680

页数：4

共 15 条

[1] Anex D. S., 1991, CHEM ENERGETIC MAT, P27
[2] SYNTHESIS AND X-RAY CRYSTAL-STRUCTURE OF 1,3,3-TRINITROAZETIDINE
ARCHIBALD, TG
GILARDI, R
BAUM, K
GEORGE, C
[J]. JOURNAL OF ORGANIC CHEMISTRY, 1990, 55 (09) : 2920 - 2924
[3] COREY EJ, 1975, TETRAHEDRON LETT, P3117
[4] CROMWELL NH, 1979, CHEM REV, V79, P336
[5] DAVIES DE, 1984, COMPREHENSIVE HETERO, V7, P237
[6] HASSNER A, 1983, HETEROCYCLIC COMPO 2, V42, P1
[7] IYER S, 1989, ARAEDTR89010 SU ARM
[8] THERMAL-DECOMPOSITION OF ENERGETIC MATERIALS .9. POLYMORPHISM, CRYSTAL-STRUCTURES, AND THERMAL-DECOMPOSITION OF POLYNITROAZABICYCLO[3.3.1]NONANES
OYUMI, Y
BRILL, TB
RHEINGOLD, AL
[J]. JOURNAL OF PHYSICAL CHEMISTRY, 1986, 90 (11) : 2526 - 2533
[9] THERMAL-DECOMPOSITION OF ENERGETIC MATERIALS .4. HIGH-RATE, INSITU, THERMOLYSIS OF THE 4, 6, AND 8 MEMBERED, OXYGEN-RICH, GEM-DINITROALKYL CYCLIC NITRAMINES, TNAZ,DNNC, AND HNDZ
OYUMI, Y
BRILL, TB
[J]. COMBUSTION AND FLAME, 1985, 62 (03) : 225 - 231
[10] 1,5-BIS(P-TOLUENESULFONYL)-3,7-DIHYDROXYOCTAHYDRO-1,5-DIAZOCINE
PAUDLER, WW
GAPSKI, GR
BARTON, JM
[J]. JOURNAL OF ORGANIC CHEMISTRY, 1966, 31 (01) : 277 - &

← 1 2 →