SYNTHESES OF L-BETA-CYANOALANINE-4-14C,L-ASPARAGINE-4-14C,AND L-ASPARTIC ACID-4-14C

被引:10
作者
GIZA, YH
RESSLER, C
机构
[1] Division of Protein Chemistry, Institute for Muscle Disease, Inc., New York, New York
来源
JOURNAL OF LABELLED COMPOUNDS | 1969年 / 5卷 / 02期
关键词
D O I
10.1002/jlcr.2590050206
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
Syntheses are described from a common labeled intermediate of β‐cyanoalanine, asparagine, and aspartic acid, each of the l configuration and labeled with carbon‐14 in carbon‐four. Radiochemical purities were 96, 99.7, and 99 %. The common source of carbon‐14 was ethyl acetyl‐dl‐β‐cyanoalaninate‐4‐14C, which was prepared from commercially available potassium cyanide‐14C by an extension of the studies of Atkinson and Hellmann and Folz. Copyright © 1969 John Wiley & Sons, Ltd.
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页码:142 / &
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