IMPROVEMENTS IN C-13 BROAD-BAND HOMONUCLEAR CROSS-POLARIZATION FOR 2D AND 3D NMR

被引：47

作者：

MOHEBBI, A ^{[1
]}

SHAKA, AJ ^{[1
]}

机构：

[1] UNIV CALIF IRVINE,DEPT CHEM,IRVINE,CA 92717

来源：

CHEMICAL PHYSICS LETTERS | 1991年 / 178卷 / 04期

基金：

美国国家科学基金会;

关键词：

D O I：

10.1016/0009-2614(91)90268-E

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

We describe a new multiple-pulse sequence (FLOPSY-8) for broadband homonuclear cross-polarization and compare it both theoretically and experimentally with the previous state of the art. FLOPSY-8 offers significant improvements in cross-polarization efficiency compared with the best alternative, and is especially useful for the large spectral bandwidths encountered in high-field carbon-13 NMR.

引用

收藏

页码：374 / 378

页数：5

相关论文

共 42 条

[21] ZERO-QUANTUM SPECTROSCOPY WITH TOCSY TRANSFER [J].

KESSLER, H ;

MRONGA, S ;

GEMMECKER, G .

JOURNAL OF MAGNETIC RESONANCE, 1990, 87 (03) :633-638

[22] NMR SEQUENTIAL ASSIGNMENT OF ESCHERICHIA-COLI THIOREDOXIN UTILIZING RANDOM FRACTIONAL DEUTERIATION [J].

LEMASTER, DM ;

RICHARDS, FM .

BIOCHEMISTRY, 1988, 27 (01) :142-150

[23] SUPERCYCLES FOR BROAD-BAND HETERONUCLEAR DECOUPLING [J].

LEVITT, MH ;

FREEMAN, R ;

FRENKIEL, T .

JOURNAL OF MAGNETIC RESONANCE, 1982, 50 (01) :157-160

[24] BROAD-BAND HETERONUCLEAR DECOUPLING [J].

LEVITT, MH ;

FREEMAN, R ;

FRENKIEL, T .

JOURNAL OF MAGNETIC RESONANCE, 1982, 47 (02) :328-330

[25] COMPOSITE PULSE DECOUPLING [J].

LEVITT, MH ;

FREEMAN, R .

JOURNAL OF MAGNETIC RESONANCE, 1981, 43 (03) :502-507

[26] PROTON NMR MEASUREMENTS OF BACTERIOPHAGE-T4 LYSOZYME AIDED BY N-15 ISOTOPIC LABELING - STRUCTURAL AND DYNAMIC STUDIES OF LARGER PROTEINS [J].

MCINTOSH, LP ;

GRIFFEY, RH ;

MUCHMORE, DC ;

NIELSON, CP ;

REDFIELD, AG ;

DAHLQUIST, FW .

PROCEEDINGS OF THE NATIONAL ACADEMY OF SCIENCES OF THE UNITED STATES OF AMERICA, 1987, 84 (05) :1244-1248

[27] RECOGNITION OF SECONDARY-STRUCTURE ELEMENTS IN 3D TOCSY-NOESY SPECTRA OF PROTEINS - INTERPRETATION OF 3D CROSS-PEAK AMPLITUDES [J].

OSCHKINAT, H ;

CIESLAR, C ;

GRIESINGER, C .

JOURNAL OF MAGNETIC RESONANCE, 1990, 86 (03) :453-469

[28] SIGN REVERSAL OF RESONANCES VIA ISOTROPIC MIXING IN NMR-SPECTROSCOPY [J].

RANCE, M .

CHEMICAL PHYSICS LETTERS, 1989, 154 (03) :242-247

[29] IMPROVED TECHNIQUES FOR HOMONUCLEAR ROTATING-FRAME AND ISOTROPIC MIXING EXPERIMENTS [J].

RANCE, M .

JOURNAL OF MAGNETIC RESONANCE, 1987, 74 (03) :557-564

[30] BROAD-BAND HOMONUCLEAR CROSS POLARIZATION IN 2D NMR USING DIPSI-2 [J].

RUCKER, SP ;

SHAKA, AJ .

MOLECULAR PHYSICS, 1989, 68 (02) :509-517

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