红外辅助蒸馏-顶空固相微萃取-气相色谱-质谱快速分析干白芷挥发油(英文)

被引：4

作者：

叶青

陈宗保

陈伟华

郑大贵

机构：

[1] 上饶师范学院江西省普通高校应用有机化学重点实验室

来源：

上饶师范学院学报 | 2010年 / 30卷 / 03期

关键词：

传统中药; 白芷; 红外蒸馏; 顶空固相微萃取; 气相色谱-质谱;

D O I：

暂无

中图分类号：

TQ461 [中草药制剂的生产];

学科分类号：

1008 ;

摘要：

采用红外辅助蒸馏-顶空固相微萃取方法萃取干白芷中的挥发油,并用气相色谱质谱方法分析了其成分,与传统的顶空固相微萃取方法比较,该方法具有萃取时间短、萃取效率高的优点,可用于干中草药挥发油的快速分析。

引用

页码：44 / 52

页数：9

共 28 条

[21]

Solid-phase microextraction on volatile components from natural grassland plants. A Cornu,A-P Carnat,B Martin,J-B Coulon,J-L Lamaison,J-L Berdaque. Journal of Agricultural and Food Chemistry . 2001

[22] Quality assessment of Flos Chrysanthemi Indici from different growing areas in China by solid-phase -: microextraction-gas chromatography-mass spectrometry [J].

Shen, S ;

Sha, YF ;

Deng, CH ;

Zhang, XM ;

Fu, DX ;

Chen, JK .

JOURNAL OF CHROMATOGRAPHY A, 2004, 1047 (02) :281-287

[23]

Solid-phase microextraction of hop volatiles for determination and verification of hop verietes. Kovacevic M,Kac M. Journal of Chromatography . 2001

[24]

Determination of baicalin and puerarinintraditional Chinese medicinal preparations by high-perfor-mance liquid chromatography. Wen K.C,Huang C.Y,Lu F.L. Journal of Chromatography A . 1993

[25]

Comparison of Essential Oil Composition of Artemisia argyi Leaves at Different Collection Times by Headspace Solid-Phase Microextraction and Gas Chromatography-Mass Spectrometry[J] . Xiaohua Zheng,Chunhui Deng,Guoxin Song,Yaoming Hu. &nbspChromatographia . 2004 (11-1)

[26]

Analysis of essential oil of radixangelicae dahuricae of supercritical fluid extraction by gas chromatog-raphy-mass spectrometry. Yang Z.J,Lei H.P,Ge F.H. Journal of Chinese Medicinal Materials . 2005

[27]

Microwave-assisted Headspace SPMEforthe Analysis of Bio-emissionsfromEu-calyptus Citriodora Leaves. Xiong G.H,Goodridge L.M,Wang Y,ChenJ. Journal of Agricultural and Food Chemistry . 2003

[28]

Analyzing of the volatile chemical constituents in Artemisia capillaris herba by GC-MS and correlative chemometric resolution methods. Guo FQ,Liang YZ,Xu CJ,et al. Journal of Chromatography A . 2004

← 1 2 3 →