香樟木质部挥发性成分的SPME-GC/MS分析

被引：11

作者：

李权 ^{[1
]}

王晓娴 ^{[1
]}

林金国 ^{[1
]}

江茂生 ^{[2
]}

初雷霞 ^{[2
]}

机构：

[1] 福建农林大学材料工程学院

[2] 福建农林大学生命科学学院

来源：

质谱学报 | 2014年 / 35卷 / 06期

关键词：

香樟; 固相微萃取; 挥发性成分; 气相色谱-质谱(GC/MS);

D O I：

暂无

中图分类号：

O657.63 [质谱分析]; TQ651.2 [];

学科分类号：

070302 ; 081704 ; 0817 ;

摘要：

采用固相微萃取技术(SPME)吸附香樟木质部挥发性成分,结合气相色谱-质谱(GC/MS)进行化学成分的分离和鉴定,同时比较不同色谱柱对分离效果的影响。结果表明:采用弱极性DB-5MS色谱柱共分离出51个组分,解析出43种挥发性成分,占总峰面积的97.04%,分离效果和所得的峰形较好于DB-WAXetr色谱柱。鉴定出含量较高的成分有:左旋-α-蒎烯(4.57%)、莰烯(2.14%),双环[3.1.0]-4-甲基-1-异丙基-2-己烯(4.16%)、β-蒎烯(2.3%)、邻异丙基甲苯(2.15%)、D-柠檬烯(7.49%)、桉叶油醇(13.85%)、樟脑(38.71%)、(R)-4-萜品醇(1.74%)、α-松油醇(2.40%)、黄樟素(2.96%)、α-荜澄茄油烯(4.36%)、1-石竹烯(1.92%)等。该方法可为香樟材在医药、食品和化学工业等方面的进一步开发和利用提供参考。

引用

页码：555 / 562

页数：8

共 19 条

[11]

Development of microwave-assisted extraction followed by headspace solid-phase microextraction and gas chromatography–mass spectrometry for quantification of camphor and borneol in Flos Chrysanthemi Indici[J] . Chunhui Deng,Yu Mao,Ning Yao,Xiangmin Zhang.Analytica Chimica Acta . 2006 (1)

[12]

Rapid analysis of essential oil from Fructus Amomi by pressurized hot water extraction followed by solid-phase microextraction and gas chromatography–mass spectrometry[J] . Chunhui Deng,Aiqin Wang,Shun Shen,Daxi Fu,Jiakuan Chen,Xiangmin Zhang.Journal of Pharmaceutical and Biomedical Analysis . 2005 (2)

[13]

In vitro anti-inflammatory and anti-oxidative effects of Cinnamomum camphora extracts[J] . Hye Ja Lee,Eun-A Hyun,Weon Jong Yoon,Byung Hun Kim,Man Hee Rhee,Hee Kyoung Kang,Jae Youl Cho,Eun Sook Yoo.Journal of Ethnopharmacology . 2005 (2)

[14]

Extraction and determination of volatile constituents of wood from Cinnamomum camphora by Agilent-GC/MS .2 Wenli P,Shanglian Z. Industrial and Information Systems (IIS),2010 2nd International Conference on . 2010

[15]

Specific induction of apoptosis by 1,8-cineole in two human leukemiacell lines, but not a in human stomach cancer cell line[J] . H. Moteki,H. Hibasami,Y. Yamada,H. Katsuzaki,K. Imai,T. Komiya.Oncology Reports . 2002 (4)

[16] Antifungal activity of the essential oil of flowerheads of garland chrysanthemum (Chrysanthemum coronarium) against agricultural pathogens [J].

Alvarez-Castellanos, PP ;

Bishop, CD ;

Pascual-Villalobos, MJ .

PHYTOCHEMISTRY, 2001, 57 (01) :99-102

[17] Headspace constituents of the tree remain of Cinnamomum camphora [J].

Miyazawa, M ;

Hashimoto, Y ;

Taniguchi, Y ;

Kubota, K .

NATURAL PRODUCT LETTERS, 2001, 15 (01) :63-69

[18]

Antiinflammatory and antinociceptive effects of 1,8‐cineole a terpenoid oxide present in many plant essential oils[J] . F. A.Santos,V. S. N.Rao.Phytother. Res. . 2000 (4)

[19]

Fungistatic properties of Essential Oil of Cinnamomum camphora[J] . A. K. Mishra,Suresh K. Dwivedi,N. Kishore,N. K. Dubey.Pharmaceutical Biology . 1991 (4)

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