Microstructure of the Sn-Cu6Sn5 fibrous eutectic and its modification by segregation

被引:28
作者
Drevet, B [1 ]
Camel, D [1 ]
Dupuy, M [1 ]
Favier, JJ [1 ]
机构
[1] CENG,SECT CARACTERISAT PHYS MAT,CEA,DTA,LETI,OPT,F-38054 GRENOBLE 9,FRANCE
关键词
D O I
10.1016/S1359-6454(96)00060-2
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
The influence of segregation due to thermal convection on the microstructure of Sn-Cu6Sn5 fibrous eutectic alloys is studied in a Bridgman type configuration. The eutectic microstructure is characterized by means of image analysis, X-ray diffraction and scanning and transmission electron microscopy. In the absence of segregation, the eutectic is regular and its growth controlled by that of the Cu6Sn5 fibers. The effect of interphases on eutectic spacing, through orientation relationships between fibers and matrix, is also evidenced. The influence of segregation can be summed up by the following effects. At first, in agreement with the Jackson and Hunt model, it leads to a variation of the eutectic spacing which results from a variation of the fiber volume fraction. Then, the spacing is much greater than the one obtained in the absence of segregation, due to a different tin growth plane and non-optimized filer/matrix orientation relationships. Finally, the absence of steady state leads to a large dispersion of the spacing associated with a microstructural disorder. Copyright (C) 1996 Acta Metallurgica Inc.
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收藏
页码:4071 / 4084
页数:14
相关论文
共 34 条
[11]  
Eustathopoulos N., 1983, International Metals Reviews, V28, P189
[12]   PERFECTION AND THERMAL-STABILITY OF LAMELLAR STRUCTURES OF PB-SN EUTECTIC [J].
FAVIER, JJ ;
TURPIN, M ;
PETIPAS, C ;
LABULLE, B .
JOURNAL OF APPLIED CRYSTALLOGRAPHY, 1977, 10 (AUG1) :213-219
[13]  
FAVIER JJ, 1980, ANN CHIM-SCI MAT, V5, P268
[14]  
FAVIER JJ, 1984, ESA, P127
[15]   X-RAY-DIFFRACTION AND CALORIMETRIC INVESTIGATION OF COMPOUND CU6SN5 [J].
GANGULEE, A ;
DAS, GC ;
BEVER, MB .
METALLURGICAL TRANSACTIONS, 1973, 4 (09) :2063-2066
[16]   GROWTH OF INTERDENDRITIC EUTECTIC IN DIRECTIONALLY SOLIDIFIED AL-SI ALLOYS [J].
GRUGEL, R ;
KURZ, W .
METALLURGICAL TRANSACTIONS A-PHYSICAL METALLURGY AND MATERIALS SCIENCE, 1987, 18 (06) :1137-1142
[17]   DEVELOPMENT OF PREFERRED ORIENTATIONS DURING FREEZING OF METALS AND ALLOYS [J].
HELLAWELL, A ;
HERBERT, PM .
PROCEEDINGS OF THE ROYAL SOCIETY OF LONDON SERIES A-MATHEMATICAL AND PHYSICAL SCIENCES, 1962, 269 (1339) :560-&
[18]  
HUNT JD, 1968, T METALL SOC AIME, V242, P1043
[19]  
JACKSON KA, 1966, T METALL SOC AIME, V236, P1129
[20]  
Kubaschewek O., 1979, METALLURGICAL THERMO, pp333