Non-destructive characterization of recrystallization kinetics using three-dimensional X-ray diffraction microscopy

被引:51
作者
Lauridsen, E. M. [1 ]
Schmidt, S.
Nielsen, S. F.
Margulies, L.
Poulsen, H. F.
Jensen, D. Juul
机构
[1] Riso Natl Lab, Ctr Fundamental Res Met Struct Four Dimens, DK-4000 Roskilde, Denmark
[2] European Synchrotron Radiat Facil, F-38043 Grenoble, France
关键词
X-ray; diffraction; 3DXRD; recrystallization; in situ;
D O I
10.1016/j.scriptamat.2006.02.028
中图分类号
TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
Three-dimensional X-ray diffraction (3DXRD) is used to characterize the nucleation and early growth of individual bulk nuclei in situ during recrystallization of 92% cold-rolled copper. It is found that some cube nuclei, but not all, have a significantly faster initial growth than the average growth kinetics. These results are discussed and compared to previous 3DXRD results for recrystallization of aluminum alloys, and implications of the results on modeling of recrystallization are considered. Finally, a new 3DXRD technique suitable for non-destructive 3D characterization is outlined and its potential for recrystallization studies is discussed. (c) 2006 Acta Materialia Inc. Published by Elsevier Ltd. All rights reserved.
引用
收藏
页码:51 / 56
页数:6
相关论文
共 29 条
  • [1] ALPERS A, IN PRESS ADV DISCRET
  • [2] DUGGAN B, 1996, ICOTOM, V11
  • [3] Non-destructive mapping of grains in three dimensions
    Fu, X
    Poulsen, HF
    Schmidt, S
    Nielsen, SF
    Lauridsen, EM
    Jensen, DJ
    [J]. SCRIPTA MATERIALIA, 2003, 49 (11) : 1093 - 1096
  • [4] Direct observation of subgrain evolution during recovery of cold-rolled aluminium
    Gundlach, C
    Pantleon, W
    Lauridsen, EM
    Margulies, L
    Doherty, RD
    Poulsen, HF
    [J]. SCRIPTA MATERIALIA, 2004, 50 (04) : 477 - 481
  • [5] Humphreys F.J., 2017, Recrystallization and Related Annealing Phenomena
  • [6] Real-time observation of grain nucleation and growth during solidification of aluminium alloys
    Iqbal, N
    van Dijk, NH
    Offerman, SE
    Moret, MP
    Katgerman, L
    Kearley, GJ
    [J]. ACTA MATERIALIA, 2005, 53 (10) : 2875 - 2880
  • [7] JENSEN DJ, 2002, P SCI TECHN INT
  • [8] Three-dimensional analysis of microstructures
    Kral, MV
    Mangan, MA
    Spanos, G
    Rosenberg, RO
    [J]. MATERIALS CHARACTERIZATION, 2000, 45 (01) : 17 - 23
  • [9] Nucleation of recrystallization observed in situ in the bulk of a deformed metal
    Larsen, AW
    Poulsen, HF
    Margulies, L
    Gundlach, C
    Xing, QF
    Huang, XX
    Jensen, DJ
    [J]. SCRIPTA MATERIALIA, 2005, 53 (05) : 553 - 557
  • [10] Lauridsen EM, 2001, RECRYSTALLIZATION AND GRAIN GROWTH, VOLS 1 AND 2, P589