TEM and SNMS studies on the oxidation behaviour of NiCrAlY-based coatings

被引:17
作者
Clemens, D [1 ]
Vosberg, VR [1 ]
Penkalla, HJ [1 ]
Breuer, U [1 ]
Quadakkers, WJ [1 ]
Nickel, H [1 ]
机构
[1] FORSCHUNGSZENTRUM JULICH, CENT CHEM DEPT, D-52425 JULICH, GERMANY
来源
FRESENIUS JOURNAL OF ANALYTICAL CHEMISTRY | 1997年 / 358卷 / 1-2期
关键词
ALLOYS; GROWTH; SCALES; OXIDE; LAYERS;
D O I
10.1007/s002160050361
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
The effect of minor Ti additions content (0% Ti, 0.4% Ti, 1% Ti, 2% Ti) on the oxidation behaviour of Ni-20Cr-10Al-0.4Y (in weight-%) model alloys was investigated in the temperature range 950 degrees C to 1100 degrees C up to 200 h in Ar - 20% O-2, Alloy microstructure, oxide scale morphology and microstructure of the scale were characterized by SEM/EDX and TEM, The growth mechanisms of the alumina scales formed on the model alloys were studied by two-stage oxidation experiments with O-18(2)-tracer and subsequent SNMS-analyses. The microstructural observations were correlated with the oxide scale properties in respect to growth rates and spalling resistance, which was tested during cyclic oxidation.
引用
收藏
页码:122 / 126
页数:5
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