Sub-Angstrom high-resolution transmission electron microscopy at 300 keV.

被引:102
作者
O'Keefe, MA
Hetherington, CJD
Wang, YC
Nelson, EC
Turner, JH
Kisielowski, C
Malm, JO
Mueller, R
Ringnalda, J
Pan, M
Thust, A
机构
[1] Univ Calif Berkeley, Lawrence Berkeley Lab, Natl Ctr Electron Microscopy, Div Mat Sci, Berkeley, CA 94720 USA
[2] Univ Oxford, Dept Mat, Oxford OX1 3PH, England
[3] FEI Co, Hillsboro, OR 97124 USA
[4] Lund Univ, SE-22100 Lund, Sweden
[5] Gatan Inc, Pleasanton, CA 94588 USA
[6] Forschungszentrum Julich, Inst Festkorperforsch, D-52425 Julich, Germany
关键词
HRTEM; contrast transfer theory; TEM characterization; exit-wave reconstruction;
D O I
10.1016/S0304-3991(01)00094-8
中图分类号
TH742 [显微镜];
学科分类号
摘要
Sub-(A) over circle ngstrom transmission electron microscopy has been achieved at the National Center for Electron Microscopy (NCEM) by a one-(A) over circle ngstrom microscope (OAM) project using software and enhanced hardware developed within a Brite-Euram project (Ultramicroscopy 64 (1996) 1). The NCEM O (A) over circleM provides materials scientists with transmission electron microscopy at a resolution better than 1 Angstrom by using extensive image reconstruction to exploit the significantly higher information limit of an FEG-TEM over its Scherzer resolution limit. Reconstruction methods chosen used off-axis holograms and focal series of underfocused images. Measured values of coherence parameters predict an information limit of 0.78 Angstrom. Images from a [110] diamond test specimen show that sub-Angstrom resolution of 0.89 Angstrom has been achieved with the OAM using focal series reconstruction. (C) 2001 Elsevier Science B.V. All rights reserved.
引用
收藏
页码:215 / 241
页数:27
相关论文
共 53 条
[1]  
ANSTIS GR, 1976, P 34 ANN M EL MICR S, P480
[2]   Design and performance of an ultra-high-resolution 300 kV microscope [J].
Bakker, H ;
Bleeker, A ;
Mul, P .
ULTRAMICROSCOPY, 1996, 64 (1-4) :17-34
[3]  
BLEEKER AJ, 1996, 54 ANN P MSA MINN MN, P418
[4]   Maximum-likelihood method for focus-variation image reconstruction in high resolution transmission electron microscopy [J].
Coene, WMJ ;
Thust, A ;
deBeeck, M ;
VanDyck, D .
ULTRAMICROSCOPY, 1996, 64 (1-4) :109-135
[5]  
COENE WMJ, 1992, 50 ANN P EMSA BOST M, P986
[6]   ELECTRON-MICROSCOPE IMAGE CONTRAST FOR THIN CRYSTALS [J].
COWLEY, JM ;
IIJMA, S .
ZEITSCHRIFT FUR NATURFORSCHUNG PART A-ASTROPHYSIK PHYSIK UND PHYSIKALISCHE CHEMIE, 1972, A 27 (03) :445-+
[7]   FOURIER IMAGES .1. THE POINT SOURCE [J].
COWLEY, JM ;
MOODIE, AF .
PROCEEDINGS OF THE PHYSICAL SOCIETY OF LONDON SECTION B, 1957, 70 (05) :486-+
[8]  
COWLEY JM, 1975, DIFFRACTION PHYSICS
[9]   Wave function reconstruction in HRTEM: The parabola method [J].
deBeeck, MO ;
VanDyck, D ;
Coene, W .
ULTRAMICROSCOPY, 1996, 64 (1-4) :167-183
[10]   ATOMIC IMAGING OF 3-2 MULLITE [J].
EPICIER, T ;
OKEEFE, MA ;
THOMAS, G .
ACTA CRYSTALLOGRAPHICA SECTION A, 1990, 46 :948-962