Sub-Angstrom high-resolution transmission electron microscopy at 300 keV.

被引:102
作者
O'Keefe, MA
Hetherington, CJD
Wang, YC
Nelson, EC
Turner, JH
Kisielowski, C
Malm, JO
Mueller, R
Ringnalda, J
Pan, M
Thust, A
机构
[1] Univ Calif Berkeley, Lawrence Berkeley Lab, Natl Ctr Electron Microscopy, Div Mat Sci, Berkeley, CA 94720 USA
[2] Univ Oxford, Dept Mat, Oxford OX1 3PH, England
[3] FEI Co, Hillsboro, OR 97124 USA
[4] Lund Univ, SE-22100 Lund, Sweden
[5] Gatan Inc, Pleasanton, CA 94588 USA
[6] Forschungszentrum Julich, Inst Festkorperforsch, D-52425 Julich, Germany
关键词
HRTEM; contrast transfer theory; TEM characterization; exit-wave reconstruction;
D O I
10.1016/S0304-3991(01)00094-8
中图分类号
TH742 [显微镜];
学科分类号
摘要
Sub-(A) over circle ngstrom transmission electron microscopy has been achieved at the National Center for Electron Microscopy (NCEM) by a one-(A) over circle ngstrom microscope (OAM) project using software and enhanced hardware developed within a Brite-Euram project (Ultramicroscopy 64 (1996) 1). The NCEM O (A) over circleM provides materials scientists with transmission electron microscopy at a resolution better than 1 Angstrom by using extensive image reconstruction to exploit the significantly higher information limit of an FEG-TEM over its Scherzer resolution limit. Reconstruction methods chosen used off-axis holograms and focal series of underfocused images. Measured values of coherence parameters predict an information limit of 0.78 Angstrom. Images from a [110] diamond test specimen show that sub-Angstrom resolution of 0.89 Angstrom has been achieved with the OAM using focal series reconstruction. (C) 2001 Elsevier Science B.V. All rights reserved.
引用
收藏
页码:215 / 241
页数:27
相关论文
共 53 条
[41]  
SCHISKE P, 1973, IMAGE PROCESSING COM, P82
[42]   Focal-series reconstruction in HRTEM: Simulation studies on non-periodic objects [J].
Thust, A ;
Coene, WMJ ;
deBeeck, MO ;
VanDyck, D .
ULTRAMICROSCOPY, 1996, 64 (1-4) :211-230
[43]   Numerical correction of lens aberrations in phase-retrieval HRTEM [J].
Thust, A ;
Overwijk, MHF ;
Coene, WMJ ;
Lentzen, M .
ULTRAMICROSCOPY, 1996, 64 (1-4) :249-264
[44]  
TURNER JH, 1997, 55 ANN P MSA CLEV OH, P1177
[45]   Residual wave aberrations in the first spherical aberration corrected transmission electron microscope [J].
Uhlemann, S ;
Haider, M .
ULTRAMICROSCOPY, 1998, 72 (3-4) :109-119
[46]  
Van Dyck D., 1990, P 12 INT C ELECT MIC, P26
[47]   Sub-angstrom structure characterisation: The Brite-Euram route towards one angstrom [J].
VanDyck, D ;
Lichte, H ;
vanderMast, KD .
ULTRAMICROSCOPY, 1996, 64 (1-4) :1-15
[48]  
Voelkl E., 1995, J MICROSC, V180, P39
[49]  
VOELKL E, 1995, ULTRAMICROSCOPY, V58, P97
[50]  
WADE RH, 1977, OPTIK, V49, P81