The synthesis of some new derivatives of calix[4]arene containing azo groups

被引：56

作者：

Deligöz, H ^{[1
]}

Ercan, N ^{[1
]}

机构：

[1] Pamukkale Univ, Fac Sci Arts, Dept Chem, TR-20017 Denizli, Turkey

来源：

TETRAHEDRON | 2002年 / 58卷 / 14期

关键词：

calyxarene; p-tert-butylcalix[4]arene; diazo calix[4]arene; diazo-coupling reaction;

D O I：

10.1016/S0040-4020(02)00156-4

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

Five new compounds p-(4-n-butyl-phenylazo)calix[4]arene (1), p-(4-phenylazophenylazo)calix[4]arene (2). p-(4-acetanilidazo)calix[4]arene (3), p-(N'-2-thiazol-2-ylsulfanylazo)calix[4]arene (4) and p-(2-thiazolazo)calix[4]arene (5) have been synthesized from calix[4]arene by diazo coupling with the corresponding aromatic amines. To elucidate the structures of the compounds elemental analyses, UV-vis, IR, H-1 and C-13 NMR spectral data have been used. (C) 2002 Elsevier Science Ltd. All fights reserved.

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页码：2881 / 2884

页数：4

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