Microwave assisted synthesis of pyrroles

被引：158

作者：

Danks, TN ^{[1
]}

机构：

[1] Univ Surrey, Dept Chem, Guildford GU2 5XH, Surrey, England

来源：

TETRAHEDRON LETTERS | 1999年 / 40卷 / 20期

关键词：

D O I：

10.1016/S0040-4039(99)00620-6

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

The synthesis of pyrroles by reaction of hexane-2,5-dione with primary amines has been shown to occur in less than 2 minutes under microwave activation. (C) 1999 Elsevier Science Ltd. All rights reserved.

引用

页码：3957 / 3960

页数：4

共 29 条

[1]

ABRAMOVITCH RA, 1992, SYNLETT, P795

[2] SYNTHESIS OF 1,4-DIHYDROPYRIDINES UNDER MICROWAVE IRRADIATION [J].

ALAJARIN, R ;

VAQUERO, JJ ;

NAVIO, JLG ;

ALVAREZBUILLA, J .

SYNLETT, 1992, (04) :297-298

[3] Microwave techniques for the synthesis and deuteration of minerals, with particular reference to scorodite, FeAsO4 center dot 2H(2)O [J].

Baghurst, DR ;

Barrett, J ;

Coleyshaw, EE ;

Griffith, WP ;

Mingos, DMP .

MINERALOGICAL MAGAZINE, 1996, 60 (402) :821-828

[4] MICROWAVE-INDUCED ORGANIC-REACTION ENHANCEMENT CHEMISTRY .4. CONVENIENT SYNTHESIS OF ENANTIOPURE ALPHA-HYDROXY-BETA-LACTAMS [J].

BANIK, BK ;

MANHAS, MS ;

KALUZA, Z ;

BARAKAT, KJ ;

BOSE, AK .

TETRAHEDRON LETTERS, 1992, 33 (25) :3603-3606

[5] Rapid synthesis of 2-cyanobenzothiazoles from N-aryliminodithiazoles under microwave irradiation [J].

Beneteau, V ;

Besson, T ;

Rees, CW .

SYNTHETIC COMMUNICATIONS, 1997, 27 (13) :2275-2280

[6] New route to 2-cyanobenzothiazoles via N-arylimino-1,2,3-dithiazoles [J].

Besson, T ;

Dozias, MJ ;

Guillard, J ;

Rees, CW .

JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1, 1998, (23) :3925-3926

[7] Expeditious routes to 4-alkoxyquinazoline-2-carbonitriles and thiocarbamates via N-arylimino-1,2,3-dithiazoles using microwave irradiation [J].

Besson, T ;

Dozias, MJ ;

Guillard, J ;

Jacquault, P ;

Legoy, MD ;

Rees, CW .

TETRAHEDRON, 1998, 54 (23) :6475-6484

[8] New route to 4-alkoxyquinazoline-2-carbonitriles [J].

Besson, T ;

Rees, CW .

JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1, 1996, (23) :2857-2860

[9]

BOSE AK, 1993, SYNLETT, P575

[10] STERICALLY-CROWDED PYRROLES [J].

BROADBENT, HS ;

BURNHAM, WS ;

OLSEN, RK ;

SHEELEY, RM .

JOURNAL OF HETEROCYCLIC CHEMISTRY, 1968, 5 (06) :757-+

← 1 2 3 →