A rational route to synthesize Bi2S3 nanorods in large scale

被引:18
作者
Chai, Duoli [1 ]
Yuan, XinSong [1 ]
Yang, BaoJun [1 ]
Qian, Yitai [2 ,3 ]
机构
[1] Hefei Univ Technol, Sch Chem Engn, Hefei 230009, Anhui, Peoples R China
[2] Univ Sci & Technol China, Hefei Natl Lab Phys Sci Microscale, Anhua 230026, Peoples R China
[3] Univ Sci & Technol China, Dept Chem, Hefei 230026, Anhui, Peoples R China
基金
中国国家自然科学基金;
关键词
Nanorods; Chemical synthesis; Scanning and transmission electron microscopy;
D O I
10.1016/j.ssc.2008.09.018
中图分类号
O469 [凝聚态物理学];
学科分类号
070205 ;
摘要
Bismuth sulfide nanorods were synthesized on a large scale via a simple self-sacrificing template route, by the direct reaction between the pre-prepared precursor metallic bismuth NT arrays and thiourea (Tu) in air at 100 degrees C for 16 h. XRD, TEM, SEM and HRTEM characterizations show that the prepared Bi2S3 samples are all phase pure and the Bi2S3 nanorods have uniform diameters of approximately 30-50 nm and lengths up to several micrometers. (C) 2008 Elsevier Ltd. All rights reserved.
引用
收藏
页码:444 / 447
页数:4
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