Moderate temperature synthesis of nanocrystalline Co3O4 via gel hydrothermal oxidation

被引：96

作者：

Jiang, Y

Wu, Y

Xie, B

Xie, Y

Qian, YT ^{[1
]}

机构：

[1] Univ Sci & Technol China, Dept Chem, Hefei 230026, Anhui, Peoples R China

[2] Univ Sci & Technol China, Struct Res Lab, Hefei 230026, Anhui, Peoples R China

来源：

MATERIALS CHEMISTRY AND PHYSICS | 2002年 / 74卷 / 02期

关键词：

moderate temperature; nanocrystalline Co3O4; gel; hydrothermal oxidation;

D O I：

10.1016/S0254-0584(01)00463-1

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

A novel gel hydrothermal oxidation route has been developed for preparation of nanocrystalline Co3O4 through the reaction between Co(OH)(2) gel and hydroperoxide in a hydrothermal system at 180 degreesC. X-ray powder diffraction (XRD) studies indicated that the product was well-crystallized cubic phase Of Co3O4 with a cell constant of a = 8.0722 Angstrom. The transmission electron micrograph (TEM) showed that the product consisted of monodispersive nanoparticles below 4 nm. (C) 2002 Elsevier Science B.V. All rights reserved.

引用

页码：234 / 237

页数：4

共 25 条

[1] Formation of lithium-cobalt spinel oxide (LixCo3-xO4) by solid-state reaction of a Li2CO3-Co3O4 powder mixture [J].