Electrochemical synthesis of copper sulfide nanoparticles

被引：17

作者：

Fotouhi, Lida ^{[1
]}

Rezaei, Maral ^{[1
]}

机构：

[1] Alzahra Univ, Dept Chem, Sch Sci, Tehran 1993891176, Iran

来源：

MICROCHIMICA ACTA | 2009年 / 167卷 / 3-4期

关键词：

Nanoparticle; Copper sulfide; Electrochemical; Synthesis; SOLVENTLESS SYNTHESIS; CUS; NANOCRYSTALS; NANORODS; FILMS;

D O I：

10.1007/s00604-009-0234-3

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

Cu2S nanoparticles were electrosynthesized by cyclic voltammetry between 0.10 and 1.50 V in the presence of polyvinylalcohol as stabilizer. The structure and nature of the resulting Cu2S poly (vinyl alcohol) composite were characterized by transmission electron microscopy and X-ray diffraction. The results show that electrochemically synthesized Cu2S nanoparticles are homogeneously dispersed and well separated from one another with a mean diameter of about 12 nm.

引用

页码：247 / 251

页数：5

共 42 条

[1] Preparation and characterization of CdS and Cu2S nanoparticle/polyaniline composite films [J].

Chandrakanthi, RLN ;

Careem, MA .

THIN SOLID FILMS, 2002, 417 (1-2) :51-56

[2] Electrosynthesis and characterisation of nanostructured palladium-polypyrrole composites [J].

Cioffi, N ;

Torsi, L ;

Sabbatini, L ;

Zambonin, PG ;

Bleve-Zacheo, T .

JOURNAL OF ELECTROANALYTICAL CHEMISTRY, 2000, 488 (01) :42-47

[3]

COLVIN VL, 1994, NATURE, V370, P354, DOI 10.1038/370354a0

[4]

Connolly S, 1999, ADV MATER, V11, P1202, DOI 10.1002/(SICI)1521-4095(199910)11:14<1202::AID-ADMA1202>3.0.CO

[5]

2-H

[6] Synthesis of CuS nanoparticles in water-in-carbon dioxide microemulsions [J].

Dong, X ;

Potter, D ;

Erkey, C .

INDUSTRIAL & ENGINEERING CHEMISTRY RESEARCH, 2002, 41 (18) :4489-4493

[7] A simple synthesis and characterization of CuS nanocrystals [J].

Gautam, UK ;

Mukherjee, B .

BULLETIN OF MATERIALS SCIENCE, 2006, 29 (01) :1-5

[8]

Gittins DI, 1999, ADV MATER, V11, P737, DOI 10.1002/(SICI)1521-4095(199906)11:9<737::AID-ADMA737>3.0.CO

[9]

2-1

[10] Preparation and optical absorption property of poly(acrylic acid)/copper sulfide nanocomposite films [J].

Gotoh, Y ;

Ohkoshi, Y ;

Nagura, M .

POLYMER JOURNAL, 2001, 33 (03) :303-305

← 1 2 3 4 5 →