Levitation apparatus for neutron diffraction investigations on high temperature liquids

We describe a new high temperature environment based on aerodynamic levitation and laser heating designed for neutron scattering experiments up to 3000 degrees C. The sample is heated to the desired temperature with three CO2 lasers from different directions in order to obtain a homogeneous temperature distribution. The apparent temperature of the sample is measured with an optical pyrometer, and two video cameras are employed to monitor the sample behavior during heating. The levitation setup is enclosed in a vacuum-tight chamber, enabling a high degree of gas purity and a reproducible sample environment for structural investigations on both oxide and metallic melts. High-quality neutron diffraction data have been obtained on liquid Y3Al5O12 and ZrNi alloy for relatively short counting times (1.5 h). (c) 2006 American Institute of Physics.