The solvates of o-acetamidobenzamide

被引:21
作者
Barnett, Sarah A. [1 ]
Tocher, Derek A. [1 ]
Vickers, Martin [1 ]
机构
[1] UCL, Dept Chem, London WC1H 0AJ, England
来源
CRYSTENGCOMM | 2006年 / 8卷 / 04期
基金
英国工程与自然科学研究理事会;
关键词
D O I
10.1039/b600288a
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
A series of six solvates of o-acetamidobenzamide have been prepared and characterized by single crystal X-ray diffraction. With the exception of the chloroform solvate, five of these, the 1-propanol, 1-butanol, 2-butanol, 1,2-dichloroethane, and 1,4-dioxane solvates are isostructural with similar unit cells and atomic positions for the o-acetamidobenzamide molecules. In all cases, the solvent molecules occupy pores within the hydrogen-bonded sheets of o-acetamidobenzamide. These molecules are readily lost when the crystals are exposed to the atmosphere.
引用
收藏
页码:313 / 319
页数:7
相关论文
共 16 条
[11]   On the inclusion of solvent molecules in the crystal structures of organic compounds [J].
Görbitz, CH ;
Hersleth, HP .
ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL SCIENCE, 2000, 56 :526-534
[12]   Isostructurality among five solvates of phenylbutazone [J].
Hosokawa, T ;
Datta, S ;
Sheth, AR ;
Brooks, NR ;
Young, VG ;
Grant, DJW .
CRYSTAL GROWTH & DESIGN, 2004, 4 (06) :1195-1201
[13]   Five new pseudopolymorphs of sym-trinitrobenzene [J].
Jetti, RKR ;
Boese, R ;
Thallapally, PK ;
Desiraju, GR .
CRYSTAL GROWTH & DESIGN, 2003, 3 (06) :1033-1040
[14]  
Nolze G, 1998, POWDER DIFFR, V13, P256
[15]  
Sheldrick G.M., 1997, SHELXS 97
[16]  
Wells A.F, 1977, Three dimensional nets and polyhedra