Recent progress of polar stationary phases in CEC and capillary liquid chromatography

被引：49

作者：

Dong, Xiaoli ^{[1
,2
]}

Wu, Ren'an ^{[1
]}

Dong, Jing ^{[1
]}

Wu, Minghuo ^{[1
]}

Zhu, Yan ^{[2
]}

Zou, Hanfa ^{[1
]}

机构：

[1] Chinese Acad Sci, Dalian Inst Chem Phys, Natl Chromatog R&A Ctr, Key Lab Separat Sci Analyt Chem, Dalian 116023, Peoples R China

[2] Zhejiang Univ, Dept Chem, Hangzhou 310003, Zhejiang, Peoples R China

来源：

ELECTROPHORESIS | 2009年 / 30卷 / 01期

关键词：

Capillary liquid chromatography; CEC; Polar stationary phase; PARTICLE-LOADED MONOLITHS; TRANSIENT-ISOTACHOPHORETIC GRADIENTS; ION-EXCHANGE PRECONCENTRATION; BONDED-SILICA PARTICLES; BOVINE SERUM-ALBUMIN; CATION-EXCHANGE; SOL-GEL; REVERSED-PHASE; HYDROPHILIC-INTERACTION; ELECTROCHROMATOGRAPHIC SEPARATION;

D O I：

10.1002/elps.200800412

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

The stationary phases including the nonpolar and polar stationary phases in microscale separations have been greatly developed. This review describes the recent progress of the polar stationary phases (PSPs) with the focus on their preparation and the interesting applications in the field of CEC and capillary liquid chromatography (CLC) covering the literatures from the middle of 2006 to the middle of 2008. The PSPs described herein were summarized into three types as open-tubular, particle-packed and monolithic stationary phases for either CEC or CLC, and the separation mechanisms are of hydrophilic interaction, chiral selection, ion-exchange and/or electrostatic interaction, etc. After overviewing the literatures published in the last 2 years, the research efforts on PSPs for CEC and CLC have been remaining in the fabrication of open-tubular and monolithic capillary columns; whereas, the research endeavor of PSPs on particulate-packed format seemed to decline most likely due to the commercial availability of various packing particles for CEC and CLC.

引用

页码：141 / 154

页数：14

共 112 条

[1] Enantioselective aptameric molecular recognition material:: Design of a novel chiral stationary phase for enantioseparation of a series of chiral herbicides by capillary electrochromatography [J].