Using thiosemicarbazide as starting material to synthesize CdS crystalline nanowhiskers via solvothermal route

被引：38

作者：

Wu, J

Jiang, Y

Li, Q

Liu, XM

Qian, YT ^{[1
]}

机构：

[1] Univ Sci & Technol China, Dept Chem, Anhui 230026, Peoples R China

[2] Univ Sci & Technol China, Struct Res Lab, Anhui 230026, Peoples R China

来源：

JOURNAL OF CRYSTAL GROWTH | 2002年 / 235卷 / 1-4期

关键词：

crystallites; cadmium compounds; sulfides; semiconducting II-VI materials;

D O I：

10.1016/S0022-0248(01)01929-7

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

Using thiosemicarbazide (NH2CSNHNH2) as starting material, we have successfully synthesized CdS crystalline nanowhiskers with typical length up to 12 mum and a width of 60 nm on average via a solvothermal route. Meanwhile, the effects of temperature, and reaction time were also discussed. The results revealed that the length of the CdS nanowires increased as the reaction time is lengthened. (C) 2002 Elsevier Science B.V. All rights reserved.

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页码：421 / 424

页数：4

相关论文

共 15 条

[1] Templated synthesis of CdS/PAN composite nanowires under ambient conditions [J].

Chen, M ;

Xie, Y ;

Chen, HY ;

Qiao, ZP ;

Zhu, YJ ;

Qian, YT .

JOURNAL OF COLLOID AND INTERFACE SCIENCE, 2000, 229 (01) :217-221

[2] A CDSSB PHOTOELECTRODE FOR PHOTOELECTROCHEMICAL APPLICATIONS [J].

DESHMUKH, LP ;

HOLIKATTI, SG ;

HANKARE, PP .

JOURNAL OF PHYSICS D-APPLIED PHYSICS, 1994, 27 (08) :1786-1789

[3] Applied physics - Nanowires: Small is beautiful [J].

Fasol, G .

SCIENCE, 1998, 280 (5363) :545-546

[4] Nonaqueous synthesis of CdS nanorod semiconductor [J].

Li, YD ;

Liao, HW ;

Ding, Y ;

Qian, YT ;

Yang, L ;

Zhou, GE .

CHEMISTRY OF MATERIALS, 1998, 10 (09) :2301-+

[5] Room temperature synthesis of metal chalcogenides in ethylenediamine [J].

Li, YD ;

Wang, ZY ;

Ding, Y .

INORGANIC CHEMISTRY, 1999, 38 (21) :4737-4740

[6] PHOTOLUMINESCENCE STUDY OF MBE-GROWN FILMS OF ZNS [J].

MCCLEAN, IP ;

THOMAS, CB .

SEMICONDUCTOR SCIENCE AND TECHNOLOGY, 1992, 7 (11) :1394-1399

[7] Very long carbon nanotubes [J].

Pan, ZW ;

Xie, SS ;

Chang, BH ;

Wang, CY ;

Lu, L ;

Liu, W ;

Zhou, MY ;

Li, WZ .

NATURE, 1998, 394 (6694) :631-632

[8] Mechanisms of the shape evolution of CdSe nanocrystals [J].

Peng, ZA ;

Peng, XG .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2001, 123 (07) :1389-1395

[9] Formation of high-quality CdTe, CdSe, and CdS nanocrystals using CdO as precursor [J].

Peng, ZA ;

Peng, XG .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2001, 123 (01) :183-184

[10] Surfactant-assisted synthesis of semiconductor nanotubes and nanowires [J].

Rao, CNR ;

Govindaraj, A ;

Deepak, FL ;

Gunari, NA ;

Nath, M .

APPLIED PHYSICS LETTERS, 2001, 78 (13) :1853-1855