Optimization of subcritical fluid extraction of seed oil from Nitraria tangutorum using response surface methodology

被引:101
作者
Liu, Zenggen [1 ,2 ]
Mei, Lijuan [1 ]
Wang, Qilan [1 ]
Shao, Yun [1 ]
Tao, Yanduo [1 ]
机构
[1] Chinese Acad Sci, Northwest Inst Plateau Biol, Key Lab Tibetan Med Res, Xining 810001, Peoples R China
[2] Univ Chinese Acad Sci, Beijing 100049, Peoples R China
关键词
Subcritical fluid extraction; Response surface methodology; Seeds oil; GC-MS; Nitraria tangutorum Bobr; SUPERCRITICAL CARBON-DIOXIDE; STATISTICAL OPTIMIZATION; ASSISTED EXTRACTION; MEDIUM COMPONENTS;
D O I
10.1016/j.lwt.2013.10.048
中图分类号
TS2 [食品工业];
学科分类号
100403 [营养与食品卫生学];
摘要
Subcritical fluid extraction (SFE) technology was used to extract oil from Nib-aria tangutorum seed. The best possible combination of extraction parameters was found using response surface methodology (RSM) in a three-variable, three-level Box-Behnken experimental design (BBD). The optimum extraction parameters were an extraction time of 40 min, an extraction pressure of 0.60 MPa, an extraction temperature of 44 degrees C and a raw material particle size of 0.45 mm. Conventional solvent extraction and supercritical CO2 fluid extraction were comparatively used. The yield of seed oil obtained using SFE was 12.92%, which was similar to or higher than the other methods. The chemical compositions of the seed oil, determined by GC-MS, indicate that its unsaturated fatty acids content was 97%. SFE proved to be an effective technique for extracting oil from N. tangutorum. (C) 2013 Elsevier Ltd. All rights reserved.
引用
收藏
页码:168 / 174
页数:7
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