Materials processing with supercritical antisolvent precipitation:: process parameters and morphology of tartaric acid

被引：43

作者：

Kröber, H ^{[1
]}

Teipel, U ^{[1
]}

机构：

[1] Fraunhofer ICT, D-76327 Pfinztal, Germany

来源：

JOURNAL OF SUPERCRITICAL FLUIDS | 2002年 / 22卷 / 03期

关键词：

supercritical fluids; crystallization; antisolvent; fine particles; PCA process;

D O I：

10.1016/S0896-8446(01)00124-3

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

Continuous precipitation with a compressed fluid antisolvent (PCA) has been used to produce fine particles of tartaric acid. Liquid solutions of tartaric acid in acetone, ethanol and methanol/ethanol mixtures have been sprayed into supercritical carbon dioxide used as antisolvent. Among the process parameters, pressure, temperature, flow rate of solvent and different nozzles have been tested. Furthermore, the effect of solute concentration was under investigation. (C) 2002 Elsevier Science B.V. All rights reserved.

引用

页码：229 / 235

页数：7

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