Polyacrylamide gel synthesis and sintering of Mg2SiO4:Eu3+ nanopowder

被引:46
作者
Hassanzadeh-Tabrizi, S. A. [1 ]
Taheri-Nassaj, E. [2 ]
机构
[1] Islamic Azad Univ, Najafabad Branch, Dept Mat Engn, Esfahan, Iran
[2] Tarbiat Modares Univ, Dept Mat Sci & Engn, Tehran, Iran
关键词
Sintering; Mg2SiO4; Chemical synthesis; Nanostructures; FORSTERITE MG2SIO4; LUMINESCENCE; POWDERS;
D O I
10.1016/j.ceramint.2013.01.056
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
081705 [工业催化]; 082905 [生物质能源与材料];
摘要
A Mg2SiO4:Eu3+ nanopowder was synthesized by a polyacrylamide gel method. In this route, the gelation of the solution is achieved by the formation of a polymer network which provides a structural framework for the growth of particles. The densification of the powders was also studied. An amorphous nanopowder was synthesized and crystallized to Mg2SiO4 after heat-treatment via a solid-state reaction at a relatively low temperature of about 700 degrees C. The powders prepared by the polyacrylamide gel method showed better sinterability than the powders synthesized by the conventional sol-gel method. The relative density of the sample was 97% at 1500 degrees C. (C) 2013 Elsevier Ltd and Techna Group S.r.l. All rights reserved.
引用
收藏
页码:6313 / 6317
页数:5
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