Characterization of poly(1-phenyl-1-silabutane) tacticity via H-1/C-13/Si-29 triple-resonance 3D-NMR

被引：25

作者：

Chai, MH ^{[1
]}

Saito, T ^{[1
]}

Pi, ZJ ^{[1
]}

Tessier, C ^{[1
]}

Rinaldi, PL ^{[1
]}

机构：

[1] UNIV AKRON, DEPT CHEM, AKRON, OH 44325 USA

来源：

MACROMOLECULES | 1997年 / 30卷 / 04期

关键词：

D O I：

10.1021/ma961534g

中图分类号：

O63 [高分子化学（高聚物）];

学科分类号：

070305 ; 080501 ; 081704 ;

摘要：

[No abstract available]

引用

页码：1240 / 1242

页数：3

共 28 条

[11] ADIABATIC PULSES FOR WIDE-BAND INVERSION AND BROAD-BAND DECOUPLING [J].

KUPCE, E ;

FREEMAN, R .

JOURNAL OF MAGNETIC RESONANCE SERIES A, 1995, 115 (02) :273-276

[12] PRECERAMIC POLYMER ROUTES TO SILICON-CARBIDE [J].

LAINE, RM ;

BABONNEAU, F .

CHEMISTRY OF MATERIALS, 1993, 5 (03) :260-279

[13] Tacticity of poly(1-chloro-1-fluoro ethylene) fluoropolymer determined using H-1/C-13/F-19 triple-resonance 3D-NMR [J].

Li, L ;

Rinaldi, PL .

MACROMOLECULES, 1996, 29 (13) :4808-4810

[14]

MORRIS GA, 1980, J AM CHEM SOC, V102, P428, DOI 10.1021/ja00521a097

[15] ENHANCEMENT OF NUCLEAR MAGNETIC-RESONANCE SIGNALS BY POLARIZATION TRANSFER [J].

MORRIS, GA ;

FREEMAN, R .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1979, 101 (03) :760-762

[16] Synthesis, thermal and mechanical properties of poly(methylphenylsilmethylene)s [J].

Ogawa, T ;

Murakami, M .

CHEMISTRY OF MATERIALS, 1996, 8 (06) :1260-1267

[17]

OGAWA T, 1995, POLYM PREPR AM CH PC, V36, P439

[18] ALKOXY-SUBSTITUTED POLY(SILYLENEMETHYLENES) - A NEW CLASS OF ALKOXY-SUBSTITUTED POLYMERS [J].

RUSHKIN, IL ;

INTERRANTE, LV .

MACROMOLECULES, 1995, 28 (14) :5160-5161

[19] Characterization of chain-end structures in diphenylphosphinyl-radical-initiated polystyrene via 3D H-1/C-13/P-31 correlation NMR [J].

Saito, T ;

Medsker, RE ;

Harwood, HJ ;

Rinaldi, PL .

JOURNAL OF MAGNETIC RESONANCE SERIES A, 1996, 120 (01) :125-128

[20]

SCHILLING CL, 1983, AM CERAM SOC BULL, V62, P912

← 1 2 3 →